食品科学 ›› 2020, Vol. 41 ›› Issue (18): 283-287.doi: 10.7506/spkx1002-6630-20190906-089

• 安全检测 • 上一篇    下一篇

青砖茶品质近红外特征光谱筛选及预测模型建立

王胜鹏,龚自明,郑鹏程,刘盼盼,滕靖,高士伟,桂安辉   

  1. (湖北省农业科学院果树茶叶研究所,湖北?武汉 430064)
  • 出版日期:2020-09-25 发布日期:2020-09-18
  • 基金资助:
    国家现代农业(茶)产业技术体系建设专项(CARS-19);湖北省农业科技创新中心创新团队项目(2016-620-000-001-032); 国家自然科学基金青年科学基金项目(31400586)

Selection of Characteristic Near Infrared Spectra and Establishment of Prediction Model for Qingzhuan Tea Quality

WANG Shengpeng, GONG Ziming, ZHENG Pengcheng, LIU Panpan, TENG Jing, GAO Shiwei, GUI Anhui   

  1. (Institute of Fruit and Tea, Hubei Academy of Agricultural Sciences, Wuhan 430064, China)
  • Online:2020-09-25 Published:2020-09-18

摘要: 应用近红外光谱技术对青砖茶品质进行快捷、无损评价。在保证样品完整的条件下获取光谱信息,通过光谱预处理、联合区间偏最小二乘法筛选特征光谱区间后进行主成分分析,再建立品质分数的Jordan-Elman?nets人工神经网络预测模型。最佳预处理方法为多元散射校正+二阶导数,特征光谱区间为4?377.6~4?751.7、4?755.6~5?129.7、6?262.7~6?633.9、7?386~7?756.3?cm-1,特征光谱区间前3?个主成分累计贡献率为99.15%,模型传递函数为tanh,模型对验证集样品的预测均方根误差为0.386,预测集决定系数为0.973;对未知样品品质的预测结果为:预测均方根误差0.393,预测集决定系数0.971。结果表明,在75.00~93.00?分青砖茶品质范围内,应用近红外光谱和Jordan-Elman?nets人工神经网络方法实现了对青砖茶品质的快速、准确评价。

关键词: 青砖茶;品质;近红外光谱;联合区间偏最小二乘法;人工神经网络

Abstract: Near infrared spectroscopy (NIRS) was used for rapid and nondestructive evaluation of the quality of Qingzhuan tea. Under the premise of ensuring the integrity of samples, spectra were acquired and preprocessed, and the characteristic spectral intervals were selected by synergy interval partial least squares?(siPLS). Furthermore, principal component analysis was performed, and a prediction model was established for the sensory evaluation score of Qingzhuan tea by Jordan-Elman back propagation-artificial neural network. The best pretreatment method was multiple scatter correction + 2nd derivative, the characteristic spectral intervals were 4 377.6–4 751.7, 4 755.6–5 129.7, 6 262.7–6 633.9, and 7 386–7 756.3 cm-1, and the cumulative contribution rate of the first three principal components in the characteristic spectral regions was 99.15%. The transfer function of the model was tanh with root mean square error of cross-validation set (RMSECV) and determinant coefficient for prediction (R2p) of 0.386 and 0.973, respectively. The root means square error and the determinant coefficient were respectively 0.393 and 0.971 for unknown Qingzhuan tea samples. The results showed that NIRS combined with Jordan-Elman back propagation-artificial neural network could allow rapid and accurate evaluation the quality of Qingzhuan tea scoring in the range of 75.00–93.00.

Key words: Qingzhuan tea; quality; near infrared spectroscopy; synergy interval partial least squares; back propagation-artificial neural network

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