食品科学 ›› 2008, Vol. 29 ›› Issue (8): 553-556.

• 分析检测 • 上一篇    下一篇

转基因油菜籽中重金属铅、镉、铜、铬、铁含量的测定

魏行, 沈敏,李胜清, 薛爱芳, 陈浩   

  1. 华中农业大学理学院化学系
  • 出版日期:2008-08-15 发布日期:2011-08-26

Determination of Pb,Cd,Cu,Cr and Fe in Transgenic Rapeseeds by Atomic Absorption Spectrometry

 WEI  Xing, SHEN  Min, LI  Sheng-Qing, XUE  Ai-Fang, CHEN  Hao   

  1. Department of Chemistry,College of Science,Huazhong Agricultural University,Wuhan 430070,China
  • Online:2008-08-15 Published:2011-08-26

摘要: 本实验对抗除草剂品种的转基因油菜籽进行湿法消解预处理,处理液采用石墨炉和火焰原子吸收光谱法进行检测,测定重金属铅、镉、铜、铬、铁的含量,并做加标回收实验。按照相同方法处理非转基因油菜籽,并测定其重金属的含量,通过比较,发现该品种的转基因油菜籽与非转基因油菜籽中这五种重金属的含量没有明显差别。

关键词: 转基因油菜籽, 重金属, 原子吸收光谱法

Abstract: A simple procedure was developed to determine contents of heavy metals in transgenic rapeseeds. After wet digestion of samples,five heavy metals,Such as Pb,Cd,Cu,Cr and Fe were determined by flame atomic absorption spectrometry(FAAS) or graphite furnace atomic absorption spectrometry(GFAAS) with regard to their concentrations,respectively. The experiments of standard addition were carried out to validate the proposed method,and good recoveries are present. According to the obtained concentrations of Pb,Cd,Cu,Cr and Fe in the transgenic rapeseeds and the non-transgenic rapeseeds,a conclusion can be made that there is no obvious difference in the contents of heavy metals between the two types of tested samples.

Key words: transgenic rapeseed, heavy metals, atomic absorption spectrometry