食品科学

• 安全检测 • 上一篇    下一篇

三唑磷在柚子茶加工过程中的残留水平变化

刘雁雨1,龚 蕾1,张耀海1,苏学素2,焦必宁1,3,4,*   

  1. 1.西南大学柑桔研究所,农业部柑桔产品质量安全风险评估实验室,
    农业部柑桔及苗木质量监督检验测试中心,重庆 400712;2.西南大学化学化工学院,重庆 400715;
    3.国家柑桔工程技术研究中心,重庆 400712;4.柑桔学重庆市重点实验室,重庆 400712
  • 出版日期:2015-12-25 发布日期:2015-12-24
  • 通讯作者: 焦必宁
  • 基金资助:

    国家现代农业(柑桔)产业技术体系建设专项(CARS-27);国家农产品质量安全风险评估重大专项(GJFP2015004);
    重庆市自然科学基金(重点)项目(cstc2013jjB80009)

Effect of Home Processing on Triazophos Residues in Pomelo Tea

LIU Yanyu1, GONG Lei1, ZHANG Yaohai1, SU Xuesu2, JIAO Bining1,3,4,*   

  1. 1. Citrus Research Institute, Laboratory of Quality and Safty Risk Assessment for Citrus Products, Quality Supervision and Testing
    Centre for Citrus and Seedling, Ministry of Agriculture, Southwest University, Chongqing 400712, China; 2. College of Chemistry
    and Chemical Engineering, Southwest University, Chongqing 400715, China; 3. National Citrus Engineering Research Center,
    Chongqing 400712, China; 4. Chongqing Municipal Key Laboratory for Citrus, Chongqing 400712, China
  • Online:2015-12-25 Published:2015-12-24
  • Contact: JIAO Bining

摘要:

为了解柚子茶加工过程中三唑磷残留的变化动态,通过田间喷施5 倍最高推荐剂量的三唑磷溶液以强化农药在柚子上的残留,然后按照柚子茶加工工艺进行加工,采用QuEChERS前处理技术结合气相色谱法检测三唑磷的含量,考察柚子茶加工过程对三唑磷残留量的影响。结果表明:三唑磷主要残留于柚的外果皮中,其残留量为全果的7.3 倍,而果肉中的残留量不足全果的3%。清洗可去除全果中28.5%的残留量;脱苦与浸糖处理均可显著降低外果皮中三唑磷的残留量,其加工因子分别为0.83和0.60;柚子茶成品中三唑磷残留量为0.18 mg/kg,最终加工因子为0.069。

关键词: 三唑磷, 柚子茶, 加工因子

Abstract:

The effect of home processing of pomelo tea on triazopho residues was investigated. The pesticide residues were
strengthened by spraying triazophos at fivefold higher dosage in the field trials and detected using Quick, Easy, Cheap,
Effective, Rugged, Safe (QuEChERS) pretreatment combined with gas chromatography (GC). The results showed that the
triazophos residues were mainly distributed in pomelo peel, in which its concentration was 7.3 times higher than that of
the whole fruit while its residues in flesh accounted for less than 3% of the total residues in the whole fruit. The washing
step decreased the concentration of triazophos in peel by 28.5%. Debittering and sugar-dipping gave significantly reduced
triazophos residues with processing factors (PFs) of 0.83 and 0.60, respectively. The whole process can reduce the residue of
triazophos to 0.18 mg/kg in pomelo tea with a PF value of 0.069.

Key words: triazophos, pomelo tea, processing factor

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