食品科学 ›› 2010, Vol. 31 ›› Issue (2): 1-5.doi: 10.7506/spkx1002-6630-201002001

• 工艺技术 •    下一篇

VE 微胶囊的制备及性质研究

马云标,周惠明,朱科学   

  1. 江南大学食品学院
  • 收稿日期:2009-03-09 修回日期:2009-08-26 出版日期:2010-01-15 发布日期:2010-12-29
  • 通讯作者: 周惠明 E-mail:hmzhou@jiangnan.edu.cn
  • 基金资助:

    “十一五”国家科技支撑计划项目(2006BAD27B04)

Preparation and Characterization of Microencapsulated Vitamin E

MA Yun-biao,ZHOU Hui-ming*,ZHU Ke-xue   

  1. School of Food Science and Technology, Jiangnan University, Wuxi 214122, China
  • Received:2009-03-09 Revised:2009-08-26 Online:2010-01-15 Published:2010-12-29
  • Contact: ZHOU Hui-ming*, E-mail:hmzhou@jiangnan.edu.cn

摘要:

以壳聚糖和麦芽糊精为壁材,通过喷雾干燥的方法制备VE 微胶囊。所得的微胶囊包埋率为89.02%,VE保留率为91.73%,水分含量为2.67%;扫描电镜(SEM)观察结果显示,VE 微胶囊表面形态以及内部结构良好,具有良好的包埋效果;差示扫描量热仪(DSC)测定得出微胶囊产品的Tg 值为41.579℃,热熔解温度Tm 为199.483℃表明产品有较好的贮藏稳定性以及较广的应用范围;并且对微胶囊在不同贮藏条件下的释放进行研究,引入Avrami's 公式对微胶囊释放进行分析,结果表明,微胶囊的释放速度在相对湿度75%的条件下要明显快于其他两种条件。

关键词: VE, 微胶囊, 扫描电镜(SEM), 差示扫描量热仪(DSC), 释放

Abstract:

Chitosan and maltodextrin were used as wall materials to prepare vitamin E microcapsules by spray drying. The encapsulation efficiency and retention ratio of vitamin E and the moisture content of microcapsules were 89.02%, 91.73% and 2.67%, respectively. Fine surface and internal structure of microcapsules were observed under scanning electron microscopy (SEM). The values of Tg and Tm of microencapsulated vitamin E were determined by DSC to be 41.579 ℃ and 199.483 ℃, respectively, indicating good storage stability and broad application range. In addition, the retention ratio of microencapsulated vitamin E was measured at different relative humidity and modeled as a function of storage temperature using Avrami’s equation. Results showed that releasing rate of vitamin E at 75% relative humidity was even faster than that at 32% or 50%.

Key words: vitamin E, microencapsulation, scanning electron microscopy (SEM), differential scanning calorimetry (DSC), release

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