食品科学 ›› 2009, Vol. 30 ›› Issue (8): 42-46.doi: 10.7506/spkx1002-6630-200908005

• 工艺技术 • 上一篇    下一篇

微波辅助水蒸汽蒸馏法和无溶剂微波萃取法提取孜然精油工艺的研究

杨艳1,吴素玲2,张卫明2,孙晓明2,张锋伦2   

  1. 1. 南京农业大学 2. 南京野生植物综合利用研究院  
  • 收稿日期:2008-06-13 修回日期:2008-11-11 出版日期:2009-04-15 发布日期:2010-12-29
  • 通讯作者: 张卫明 E-mail:botanyzh@163.com
  • 基金资助:

    “十一五”国家科技支撑计划项目(2006BAD06B02)

Study on Microwave-assisted Hydrodistillation Extraction and Solvent-free Microwave Extraction of Essential Oil from Cumin (Cuminum cyminum L.) Seed

YANG Yan1,WU Su-ling2,ZHANG Wei-ming2,*,SUN Xiao-ming2,ZHANG Feng-lun2   

  1. (1. Nanjing Agricultural University, Nanjing 210095, China;
    2. Nanjing Institute of Comprehensive Utilization ofWild Plants, Nanjing 210042, China)
  • Received:2008-06-13 Revised:2008-11-11 Online:2009-04-15 Published:2010-12-29
  • Contact: ZHANG Wei-ming2,*, E-mail:botanyzh@163.com

摘要:

采用微波蒸馏法提取孜然精油,考察微波溶剂提取和无溶剂提取孜然精油工艺中微波提取时间、微波功率、粒度和液料比等因素对孜然精油提取率的影响。同时以枯茗醛含量作为精油品质的评价指标,并通过GC对孜然精油进行分析。研究结果表明,微波溶剂提取孜然精油的最佳工艺条件为:液料比6:1、微波提取时间90min、微波功率300W,此条件下精油提取率为3.501%,精油中枯茗醛含量为19.121%。微波无溶剂提取孜然精油的最佳工艺条件为:浸泡时间30min、微波提取时间45min、微波功率200W,此条件下精油提取率为2.461%,精油中枯茗醛含量为23.910%。

关键词: 微波, 精油, 枯茗醛

Abstract:

The microwave-assisted hydrodistillation (MAHD) and solvent-free microwave extraction (SFME) processes of essential oil from cumin seed were optimized through orthogonal test respectively, and the quality of essential oil was analyzed by GC with the content of cuminaldehyde as the evaluation index. Results showed that the optimum conditions of MAHD extraction are as follows: extraction time 90 min, microwave power 300 W, ratio of solvent to raw material 6:1, and under these conditions the extraction yield and the content of cuminaldehyde are 3.501% and 19.121%, respectively. The optimum conditions of SFME extraction are as follows: extraction time 45 min, soaking time 30 min, microwave power 200 W, and under these conditions the extraction yield and the content of cuminaldehyde are 2.461% and 23.910%, respectively.

Key words: microwave, essential oil, cuminaldehyde

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