食品科学 ›› 2011, Vol. 32 ›› Issue (6 ): 104-109.doi: 10.7506/spkx1002-6630-201106023

• 工艺技术 • 上一篇    下一篇

地黄叶浸膏微波真空低温干燥工艺优化

王 莹,李页瑞,王 翔,刘砚墨,刘雪松,王龙虎,陈 勇*   

  1. 浙江大学药学院
  • 收稿日期:2010-07-02 修回日期:2011-01-24 出版日期:2011-03-25 发布日期:2011-03-03
  • 通讯作者: 李页瑞 E-mail:leecoyr@zju.edu.cn
  • 基金资助:
    温州市龙湾区科技发展计划项目(2008SIZ)

Optimization of Microwave Vacuum Low-temperature Drying Process for Rehmannia glutinosa Libosch Leaves Extract

WANG Ying,LI Ye-rui,WANG Xiang,LIU Yan-mo,LIU Xue-song,WANG Long-hu,CHEN Yong*   

  1. College of Pharmaceutical Sciences, Zhejiang University, Hangzhou 310058, China
  • Received:2010-07-02 Revised:2011-01-24 Online:2011-03-25 Published:2011-03-03
  • Contact: LI Ye-rui E-mail:leecoyr@zju.edu.cn

摘要: 为充分利用地黄叶资源,提高其经济附加值并为植物提取物干燥提供方法。采用单因素试验考察微波功率、干燥时间等因素对干燥产物含水率的影响,在单因素试验的基础上,选用L9(34)正交试验法和多指标综合评分法对工艺参数进行优化,确定地黄叶浸膏微波真空低温干燥的最佳工艺条件,并与真空烘箱干燥、真空带式干燥和冷冻干燥等方法进行比较研究。结果表明:地黄叶浸膏微波真空低温干燥的最佳工艺条件为浸膏初始含水率45%、微波功率2kW、干燥时间18min、装料盘转速90r/min、间歇比3:1、装载量110g;在此工艺条件下干燥产物含水率2.89%、毛蕊花糖苷保留率95.98%、地黄叶总苷保留率89.41%。与其他干燥方法相比,微波真空干燥具有干燥产品含水率低、有效成分损失少、干燥时间短且操作简便等优点,工艺稳定可靠,有较大的工业化应用价值。

关键词: 地黄叶, 微波真空低温干燥, 毛蕊花糖苷, 地黄叶总苷, 多指标综合评分

Abstract: In order to make full utilization of Rehmannia glutinosa Libosch leaf resource, improve its added value and provide optimal drying method for Rehmannia glutinosa Libosch leaves extract, single-factor design was used to explore the effects of microwave power and drying time on water content of dried products, followed by process optimization for the microwave vacuum drying of the extract by orthogonal array design based on multi-index comprehensive evaluation. Results indicated that the optimal microwave vacuum drying parameters were initial water content in extract of 45%, microwave power of 2 kW, heating time of 18 min, rotating speed for loading tray of 90 r/min, intermittent ratio of 3:1 and loading amount of 110 g. Under the optimal drying conditions, water content, retention rate of verbascoside and retention rate of total glycosides were 2.89%, 95.98% and 89.41%, respectively. Compared with vacuum oven drying, vacuum belt drying and freeze drying, microwave vacuum drying has the remarkable advantages of low water content, less loss rate of bioactive components, short drying time, high retention rate of bioactive components and simple operation, which exhibits promising application value in the field of industry due to its stability and reliability.

Key words: Rehmannia glutinosa Libosch leaves, microwave vacuum drying process, verbascoside, total glycosides, multi-index comprehensive evaluation

中图分类号: