食品科学 ›› 2010, Vol. 31 ›› Issue (14 ): 148-152.doi: 10.7506/spkx1002-6630-201014033

• 工艺技术 • 上一篇    下一篇

水不溶性豆渣膳食纤维改性的工艺优化

田 成1,莫开菊1,2,汪兴平1,2,*   

  1. 1.湖北民族学院生物科学与技术学院 2.生物资源保护与利用湖北省重点实验室
  • 收稿日期:2010-06-25 出版日期:2010-07-15 发布日期:2010-12-29
  • 通讯作者: 汪兴平 E-mail:hbmywxp@163.com
  • 基金资助:

    湖北省科技攻关项目(2006AA201C61);湖北省教育厅项目(Q200729001)

Modification Optimization of Insoluble Dietary Fiber from Soybean Dregs

TIAN Cheng1,MO Kai-ju1,2,WANG Xing-ping1,2,*   

  1. 1. School of Biological Science and Technology, Hubei University for Nationalities, Enshi 445000, China;
    2. Key Laboratory of Biologic Resources Protection and Utilization of Hubei Province, Enshi 445000, China
  • Received:2010-06-25 Online:2010-07-15 Published:2010-12-29
  • Contact: WANG Xing-ping1, E-mail:hbmywxp@163.com

摘要:

为研究磷酸盐改性水不溶性豆渣膳食纤维的工艺条件及膳食纤维结构,以持水性作为特征性考察指标,通过单因素试验、正交试验优化其改性的工艺条件,通过X 射线衍射及电镜观察膳食纤维的结构。结果表明:水不溶性豆渣膳食纤维改性的最佳工艺参数为磷酸氢二钠溶液质量浓度0.1g/100mL、料液比1:60(g/mL)、处理时间1h、处理温度50℃,此条件下的膳食纤维持水性达11.95g/g;磷酸盐改性水不溶性豆渣膳食纤维的结构得到部分改善,表面略有褶皱,结构疏松,带有明显的片状结构,颗粒的表面出现蜂窝状结构,且分布均匀,改性后的水不溶性豆渣膳食纤维在34.76°出现较明显的衍射强度峰,其结晶度为30.57%。

关键词: 豆渣, 膳食纤维, 溶解性, 改性, 工艺优化, 结构特性

Abstract:

The phosphate modification of insoluble dietary fiber (IDF) from soybean dregs was optimized by single factor and orthogonal array design methods for maximizing its water-binding capacity (WBC). Meanwhile, the structure of modified soybean IDF was observed using X-ray diffraction and scanning electron microscopy. It was found that the optimum conditions for soybean IDF modification were as follows: disodium hydrogen phosphate concentration 0.1 g/100 mL, material/liquid ratio 1:60 (g/mL) and modification temperature 50 ℃ for a modification duration of 1 h and that the WBC of modified soybean IDF under these optimum conditions was up to 11.95 g/g. After phosphate modification, the structure of soybean IDF was improved partially and the surface became slightly wrinkled and loose and displayed distinct sheeting structure. What’s more, an evenly distributed honeycomb-like surface structure of modified soybean IDF granules was observed. The X-ray diffraction pattern of modified soybean IDF showed a remarkable intensity peak at 34.76 ℃, with a crystallinity of 30.57%.

Key words: soybean dregs, dietary fiber, solubility, modification, process optimization, structural features

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