食品科学 ›› 2009, Vol. 30 ›› Issue (17 ): 79-83.doi: 10.7506/spkx1002-6630-200917017

• 基础研究 • 上一篇    下一篇

农家腊肉冷熏加工过程中挥发性风味物质的变化

尚永彪1 , 2,吴金凤1,夏杨毅1 , 2,屠大伟3   

  1. 1.西南大学食品科学学院 2.重庆市特色食品工程技术研究中心 3.重庆市计量质量检测研究院
  • 收稿日期:2009-05-03 出版日期:2009-09-01 发布日期:2014-04-14
  • 通讯作者: 尚永彪 E-mail:shangyb@sohu.com
  • 基金资助:

    “十一五”国家科技支撑计划项目(2007BAD51B06);重庆市特色食品工程技术研究中心项目

Changes of Volatile Flavor Compounds in Traditional Chinese Bacon during Cold Smoking

SHANG Yong-biao1,2,WU Jin-feng1,XIA Yang-yi1,2,TU Da-wei3   

  1. 1. College of Food Science, Southwest University, Chongqing 400716, China;
    2. Specialty Research Technology Center of Food Engineering in Chongqing, Chongqing 400716, China;
    3. Chongqing Academy of Metrology and Quality Inspection, Chongqing 400020, China
  • Received:2009-05-03 Online:2009-09-01 Published:2014-04-14
  • Contact: SHANG Yong-biao E-mail:shangyb@sohu.com

摘要:

以重庆农家腊肉为对象,研究冷熏加工过程中挥发性物质的变化规律,以期为传统特色腊肉产品的工艺改进提供理论依据。采用同时蒸馏萃取法(SDE)结合气质联用仪(GC-MS)、以癸酸乙酯为内标,分别对腌制结束、烟熏与烘烤10、20、30d 后农家腊肉生产过程中4 个阶段挥发性风味成分的变化进行定性和半定量分析。实验结果表明:4 个阶段腊肉中挥发性成分的种类分别为:40、59、68 和72 种;腊肉中挥发性物质的相对含量百分数变化分别为:酚类从0 增加到33.19%,醇类从21.94% 减少到13.74%,醚类从3.84% 减少到0.88%,羰基类从13.99% 减少到8.88%,酸类从1.26% 增加到2.55%,酯类从27.32% 减少到24.96%,碳氢化合物从5.71% 增加到12.69%;通过对挥发性风味物质的定性分析,确定了腊肉中主体风味物质为酚类、羰基类、醇类、酯类和碳氢化合物。

关键词: 腊肉, 挥发性风味成分, 同时蒸馏萃取, 气质联用

Abstract:

In order to make clear the formation mechanism and pathways of flavor substances, the changes of main volatile flavor compounds in Chongqing traditional Chinese bacon during cold smoking were analyzed. SDE combined with GC-MS was adopted for the qualitative and semiquantitative determination of volatile compounds in dry-cured and 10, 20 and 30 d smoked bacon samples using ethyl caprate as an internal standard. Only 40 volatile compounds were identified from the dry-cured bacon samples, while 59, 68, and 72 compounds were identified from 10, 20 and 30 d smoked bacon samples, respectively. The relative contents of phenols, acids and hydrocarbons increased obviously (from 0 to 33.19%, 1.26% to 2.55% and 5.71% to 12.69 %, respectively). In contrast, carbonyls (13.99% to 8.88 %), esters (27.32% to 24.96 %), alcohols (21.94% to 13.74 %) and ethers (3.84% to 0.88 %) experienced a decrease during cold smoking (the process of smoking dry cured bacon for 30 d). The main flavor compounds in Chongqing traditional bacon were phenols, carbonyls, alcohols, esters and hydrocarbons.

Key words: traditional Chinese bacon, volatile flavor compound, SDE, GC-MS

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