食品科学 ›› 2008, Vol. 29 ›› Issue (4): 306-309.

• 分析检测 • 上一篇    下一篇

抑制型离子色谱同时测定分离检测鱼酱油中的九种有机酸(英文)

 徐伟, 于刚, 薛长湖, 任艳, 高瑞昌   

  1. 中国海洋大学食品科学与工程学院; 中国海洋大学食品科学与工程学院;
  • 出版日期:2008-04-15 发布日期:2011-08-24

Simultaneous Determination of Nine Kinds of Fish Sauce Organic Acids by Ion Chromatography with Suppressed Conductivity Detection

 XU  Wei, YU  Gang, XUE  Chang-Hu, REN  Yan, GAO  Rui-Chang   

  1. College of Food Science and Engineering, Ocean University of China
  • Online:2008-04-15 Published:2011-08-24

摘要: 建立了用亲水性阴离子交换分离柱,KOH为淋洗液作梯度淋洗,电导检测,同时分离和检测鱼酱油中九种有机酸的离子色谱法。方法对所测有机酸的线性范围均在2个数量级以上,回收率在93.65%~104.32%之间,该方法用于鱼酱油样品的分析结果显示具有准确、高效、回收率高和重现性好的特点。

关键词: 离子色谱, 有机酸, 鱼酱油

Abstract: A method for the determination of nine kinds of fish sauce organic acids was developed by ion chromatography with suppressed conductivity detection. The separation of the organic acids was achieved on hydrophilic anion exchange column with potassium hydroxide as gradient eluent with gradient pump. The detection was performed by a conductivity detection mode. The calibration graphs of peak area for all analytes were linear in the ranges about two orders of magnitude. The recoveries of addition standard are within 93.65 %~104.32 %. The results indicated that this method is highly accurate and efficient with good reproducibility and high recovery.

Key words: ion chromatography, organic acid, fish sauce