食品科学 ›› 2006, Vol. 27 ›› Issue (12): 322-325.

• 工艺技术 • 上一篇    下一篇

湘西产枳椇籽亚麻酸超临界CO2萃取研究

卢成英,雷华平,张敏,黄早成,刘立平   

  1. 吉首大学林产化工工程湖南省重点实验室;
  • 出版日期:2006-12-15 发布日期:2011-11-23

Study on the Supercritical CO2 Extraction of Hovenia acerba Seed Fatty Acids

LU Cheng-ying,LEI Hua-ping,ZHANG Min,HUANG Zao-cheng,LIU Li-ping   

  1. Key Laboratory for Forest Products Chemical Industry Engineering of Hunan, Jishou University, Zhangjiajie 427000, China
  • Online:2006-12-15 Published:2011-11-23

摘要: 探索超临界CO2流体技术萃取湘西产枳椇籽亚麻酸的最佳条件,并对枳椇籽脂肪酸提取物进行了理化检测。研究表明超临界CO2萃取最佳条件为萃取温度45℃、压力36MPa、时间120min、分离釜Ⅰ压力10MPa,此条件下提取脂肪酸得率为8.1%,α-亚麻酸相对含量为37.90%。GC-MS分析显示超临界CO2萃取的枳椇籽油主要脂肪酸组分为α-亚麻酸、油酸、亚油酸、棕榈酸和硬脂酸,其中不饱和脂肪酸的相对含量为74.76%。

关键词: 枳椇籽, 超临界萃取, &alpha, -亚麻酸, GC-MS

Abstract: The fatty acids of the Hovenia acerba seed were extracted using the supercritical CO2 extraction technique. Also GC and GC-MS was used to detect the quality of the seed oil. The optimized supercritical CO2 extraction conditions are as follows: an extraction pressure of 36MPa, an extraction temperature of 45℃, an extraction time of 120min, a separatorⅠpressure of 10MPa. with a crude fat yield of 8.1% and a linolenic acid content of 37.90%. The GC-MS analysis showed that the dominant fatty acids in the oil are α-Linolenic, oleic acid, linoleic ,palmitic acid, stearic acid, etc. The content of PUFA in the product is 74.76%.

Key words: Hovenia acerba; supercritical fluid extraction (SFE); &alpha, -Linolenic; GC-MS;