食品科学 ›› 2003, Vol. 24 ›› Issue (4): 128-132.

• 分析检测 • 上一篇    下一篇

近红外光谱在淀粉糖生产中的应用

 杨维旭, 张显友, 王雁飞, 高春华   

  1. 吉林燃料乙醇有限责任公司质检中心,吉林中西医结合医院药剂科
  • 出版日期:2003-04-15 发布日期:2011-12-13

The Application of Near-infrared Spectroscopyin Starch-sugar Production

 YANG  Wei-Xu, ZHANG  Xian-You, WANG  Yan-Fei, GAO  Chun-Hua   

  • Online:2003-04-15 Published:2011-12-13

摘要: 本文论述了采用近红外光谱漫反射技术检测葡萄糖浆中主要成分含量的方法。讨论了采用偏最小二乘法(PLS)建立校正模型过程中样品预处理及利用常规吸收峰优选波长的方法。经验证:DE、DP分布测量值同浓度参考值具有良好相关性(相关系数大于0.9),测量重复性变异系数(CV)优于2%。结果表明:近红外光谱法可以满足葡萄糖浆中主要成分的实际测量要求,为玉米深加工企业提供了淀粉糖生产过程控制的参考方法。

关键词: 葡萄糖值, DP分布, 近红外光谱, 偏最小二乘法, 基础数据, 定标模型

Abstract: The method of assay of principal constituents of Glucose slurry by r eflectance technicology of Near-infrared spectroscopy has been expounded in thi s thesis. The authors has described the pre-treatment way of sample during the period of setting regression models by partial least-squares(PLS) and the way o f wavelength optimum selection according to normal absorbing peak .It’s test a nd verified that the measuring value of DE and DP has a good correlation betw ee n prediction values with reference values (correlation coefficient is higher th an 0.9), In addition,the results were reliable with coefficient of variation (CV ) of repeatability below 2 percent. Therefore, Near-infrared spectroscopy o f r eflectance technicology could meet practical measurement accuracy as require d fo r principal constituents of Glucose slurry. This study provided a new refer ence method to control starch-sugar procedure for those companies engaged in d eep-process industry.

Key words: dextrose equivalent, distributing polymerization, Near-infrared spe ctroscopy, partial least-squares(PLS), basedata, quantitative model