响应面法微波辅助乙醇提取红景天苷工艺优化

doi:10.7506/spkx1002-6630-201314030

食品科学

响应面法微波辅助乙醇提取红景天苷工艺优化

赵子铭，付刚，李诚

1.四川农业大学生命科学与理学院，四川雅安 625014；2.四川农业大学食品学院，四川雅安 625014

出版日期:2013-07-25 发布日期:2013-08-02

Optimization of Microwave-Assisted Extraction of Salidroside from Rhodida rosea by Response Surface Methodology

ZHAO Zi-ming，FU Gang，LI Cheng

1. College of Life and Basic Sciences, Sichuan Agricultural University, Ya’an 625014, China；
2. College of Food Science, Sichuan Agricultural University, Ya’an 625014, China

Online:2013-07-25 Published:2013-08-02

摘要/Abstract

摘要：

对红景天中红景天苷微波辅助乙醇提取工艺进行优化，并用高效液相色谱法检测红景天苷含量。实验先采用单因素试验分析原料粒度、微波时间、微波功率、乙醇体积分数、浸提温度、浸提时间、液料比7个因素对红景天苷提取率影响，再采用四因素三水平响应面分析法进行试验，并对各个因素的显著性和交互作用进行分析。结果表明：最优工艺条件为原料粒度40目、微波时间42s、微波功率480W、乙醇体积分数78%、提取温度72℃、浸提时间90min、液料比10:1(mL/g)，此条件下红景天苷提取率为93.53%。

关键词: 红景天苷, 提取工艺, 优化, 响应面法

Abstract:

The process conditions for microwave-assisted extraction of salidroside from Rhodida rosea were optimized.
HPLC was used to detect salidroside. The effects of seven process parameters including material particle size, microwave
treatment time, microwave power, alcohol concentration, extraction temperature, extraction time and solid-liquid ratio on
the extraction rate of salidroside were investigated through single factor tests. The significance and interaction effects of
microwave treatment time, microwave power, ethanol concentration and extraction temperature were analyzed by response
surface analysis based on a three-level central composite design. The optimal microwave-assisted extraction conditions for
salidroside were achieved to be microwave treatment duration of 42 s, microwave power of 480 W, ethanol concentration of
78%, solid-liquid ratio of 1:10 (g/mL) and extraction temperature of 72 ℃, extraction time of 90 min and material particle
size of 40 mesh. Under these extraction conditions, the extraction rate of salidroside from Rhodida rosea was up to 93.53%.

Key words: salidroside, extraction process, optimization, response surface methodology

赵子铭，付刚，李诚. 响应面法微波辅助乙醇提取红景天苷工艺优化[J]. 食品科学, doi: 10.7506/spkx1002-6630-201314030.

ZHAO Zi-ming，FU Gang，LI Cheng. Optimization of Microwave-Assisted Extraction of Salidroside from Rhodida rosea by Response Surface Methodology[J]. FOOD SCIENCE, doi: 10.7506/spkx1002-6630-201314030.

[1]	王凤，肖楚翔，刘淑珍，王凤舞. 榴莲核黄酮的提取及其对秀丽隐杆线虫氧化和衰老的影响[J]. 食品科学, 2021, 42(9): 123-129.
[2]	陈茏，杨俊，马毛毛，吴莎莎，余平，曾哲灵. 产蛋白酶菌株的筛选及以菜籽粕为氮源的产酶条件优化[J]. 食品科学, 2021, 42(4): 115-121.
[3]	柳萌，郜海燕，房祥军，吴伟杰，陈杭君，刘瑞玲. 不同成熟度杨梅酚酸的超声-微波协同优化提取及其抗氧化性对比[J]. 食品科学, 2021, 42(3): 112-120.
[4]	马永强，修伟业，黎晨晨，王艺錡，陈俊杰. 星点设计-响应面法优化番茄红素纳米结构脂质载体的制备[J]. 食品科学, 2021, 42(3): 121-127.
[5]	潘飞，赵磊，陈艳麟，郝帅，张会敏. 壳聚糖/γ-聚谷氨酸负载黑米花色苷纳米粒的制备、表征及缓释性能[J]. 食品科学, 2021, 42(10): 38-44.
[6]	郭燕，邓杰，任志强，黄治国，卫春会，黄明才. 响应面优化酿酒酵母与窖泥酯化细菌协同发酵产丁酸乙酯和己酸乙酯[J]. 食品科学, 2021, 42(10): 209-217.
[7]	周志强，马金菊，甘瑾，李坤，李凯，张雯雯，涂行浩，杜丽清，张弘. 漂白紫胶/单宁酸复配涂膜对芒果常温贮藏的保鲜效果[J]. 食品科学, 2020, 41(9): 145-152.
[8]	张英昊，薛照阳，赵廷彬，殷海松，乔长晟,. 出芽短梗霉发酵液中聚苹果酸定量近红外模型的建立与应用[J]. 食品科学, 2020, 41(8): 152-158.
[9]	苏佳佳，杨天，佟恩杰，赵雪莹，何程豪，杨哪，徐学明，吴凤凤. 糙米酒酿工艺优化与挥发性成分分析[J]. 食品科学, 2020, 41(8): 177-185.
[10]	张姗姗，李晓彬，张轩铭，韩利文，刘可春. 香螺肽脱色工艺及其抗氧化活性[J]. 食品科学, 2020, 41(6): 252-258.
[11]	焦雯姝，关嘉琦，史佳鹭，李柏良，陆婧婧，闫芬芬，李娜，占萌，霍贵成. 响应面法优化乳酸乳球菌KLDS4.0325产叶酸的培养基成分及发酵条件[J]. 食品科学, 2020, 41(6): 123-130.
[12]	徐尉力，付壮，王旭，赵悦，王晨兆，马佳骏，王志兵. 沉积固化离子液体均相液液微萃取-高效液相色谱法测定蔬菜中的苯脲类农药残留[J]. 食品科学, 2020, 41(4): 248-255.
[13]	宋一凡，陈海峰，袁越锦. 猕猴桃CO2-低温高压渗透膨化干燥工艺优化[J]. 食品科学, 2020, 41(4): 229-234.
[14]	郭浩男，张莉力，冯琳琳，王天琪，王成，赵昕琪，许云贺. 结合淀粉活性乳酸菌利用生淀粉产酶条件及代谢产物[J]. 食品科学, 2020, 41(24): 46-53.
[15]	司阔林，徐捐捐，岳田利，袁亚宏，郭春锋. 布氏乳杆菌产γ-氨基丁酸发酵条件的优化[J]. 食品科学, 2020, 41(2): 87-93.

响应面法微波辅助乙醇提取红景天苷工艺优化

Optimization of Microwave-Assisted Extraction of Salidroside from Rhodida rosea by Response Surface Methodology

RichHTML

PDF (PC)

可视化

摘要/Abstract

引用本文

使用本文

参考文献

相关文章 15

编辑推荐

Metrics

本文评价