微波条件下纸包装油墨中增塑剂向食品（模拟物）的迁移

食品科学

微波条件下纸包装油墨中增塑剂向食品（模拟物）的迁移

高松，王志伟，胡长鹰

1.江南大学机械工程学院，江苏无锡 214122；2.产品包装与物流广东普通高校重点实验室，广东珠海 519070；
3.暨南大学包装工程研究所，广东珠海 519070；4.暨南大学食品科学与工程系，广东广州 510632

出版日期:2014-02-13 发布日期:2014-03-17

Migration of Plasticizers from Paper Packaging Inks to Food (Simulant) under Microwave Heating

GAO Song, WANG Zhi-wei, HU Chang-ying

1. School of Mechanical Engineering, Jiangnan University, Wuxi 214122, China; 2. Key Laboratory of Product Packaging and
Logistics for Guangdong Higher Education Institutes, Zhuhai 519070, China; 3. Packaging Engineering Institute, Jinan University,
Zhuhai 519070, China;4. Department of Food Science and Engineering, Jinan University, Guangzhou 510632, China

Online:2014-02-13 Published:2014-03-17

摘要/Abstract

摘要：

研究纸张印刷油墨中4 种增塑剂（3 种邻苯二甲酸酯类增塑剂和近年流行的环保增塑剂乙酰基柠檬酸三丁酯）向食品模拟物Tenax和奶粉的迁移，考察其在110、250、440、600、900 W微波功率下的迁移行为，探讨迁移影响因素，并与常规条件下的迁移行为做比较。结果显示在一定条件下微波功率越高，迁移量越大；且迁移行为受增塑剂的分子质量、极性等性质的影响；常规条件下的迁移影响因素也适用于微波条件。

关键词: 油墨, 增塑剂, 纸包装, 迁移, Tenax, 奶粉

Abstract:

The migration of plasticizers from the printing inks through packaging paper to Tenax and milk powder was
studied under microwave heating at power levels of 110, 250, 440 W and 900 W, respectively, and for different contact times
ranging from 2 min at 900 W to 15 min at 110 W. The inks were offset printed by simulating the real situation, which has
never been used in migration research. The plasticizers investigated included the commonly used dibutyl phthalate (DBP),
bis(2-ethylhexyl) phthalate (DEHP), di-n-octyl phthalate (DOP) and a new type environmentally-friendly plasticizer, acetyl
tributyl citrate (ATBC). Gas chromatograph coupled with mass spectrometer (GC-MS) was used for the determination of
ethanol extracts of these plasticizers from printed paper, Tenax and milk powder. The results showed that heating power,
contact time and some properties of the compounds were all able to affect their real mass transfer. Migration factors under
the conventional conditions also apply to microwave conditions.

Key words: inks, plasticizers, paper packaging, migration, Tenax, milk powder

高松，王志伟，胡长鹰. 微波条件下纸包装油墨中增塑剂向食品（模拟物）的迁移[J]. 食品科学.

GAO Song, WANG Zhi-wei, HU Chang-ying. Migration of Plasticizers from Paper Packaging Inks to Food (Simulant) under Microwave Heating[J]. FOOD SCIENCE.

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