食品科学

• 工艺技术 • 上一篇    下一篇

牡丹籽油亚临界流体萃取工艺优化

姚茂君,李 静   

  1. 吉首大学化学化工学院,湖南 吉首 416000
  • 出版日期:2014-07-25 发布日期:2014-08-26
  • 基金资助:

    国家发改委国家生物医药高技术产业化项目(发改委高技[2007]2490号)

Optimization of Subcritical Fluid Extraction of Oil from Tree Peony (Paeonia suffruticosa Andr.) Seeds

YAO Mao-jun, LI Jing   

  1. College of Chemistry and Chemical Engineering, Jishou University, Jishou 416000, China
  • Online:2014-07-25 Published:2014-08-26

摘要:

采用亚临界流体技术萃取牡丹籽油,通过正交试验对制油工艺进行优化,并对此法所得牡丹籽油的脂肪酸
组成及理化性质进行分析。结果表明,最优萃取工艺条件为萃取温度50 ℃、萃取压强0.5 MPa、每次萃取30 min、
萃取3 次,该条件下牡丹籽出油率达24.16 %。所得牡丹籽油共鉴定出12 种脂肪酸,主要为亚麻酸(45.412 2%)、
亚油酸(38.119 9%)、棕榈酸(11.124 6%)和硬脂酸(3.648 9%)。其理化指标为:相对密度0.901 3、折光指数
1.474 2、酸值3.25 mg KOH/g、碘值175 g I2/100 g、皂化值176 mg KOH/g、过氧化值1.48 meq/kg。

关键词: 牡丹籽油, 理化性质, 脂肪酸组成, 亚临界流体

Abstract:

An orthogonal array design was employed to optimize the subcritical fluid extraction of seed oil from tree peony
(Paeonia suffruticosa Andr.). The fatty acid composition and physicochemical properties of the seed oil were analyzed. The
results showed that the optimum extraction conditions were determined to be extraction at 50 ℃ and 0.5 MPa performed
three times for 30 min each, resulting in an oil yield of 24.16%. Twelve fatty acids were identified in the extracted seed oil
and the major fatty acids were linolenic acid (45.412 2%), linoleic acid (38.119 9%), palmitic acid (11.124 6%) and stearic
acid (3.648 9%). The physicochemical indexes were as follows: relative density 0.901 3, index of refraction 1.474 2, acid
value 3.25 mg/g, iodine value 175 g/100 g, saponification value 176 mg/g, and peroxide value 1.48 meq/kg.

Key words: tree peony seed oil, physicochemical properties, fatty acid composition, subcritical fluid extraction

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