食品科学

• 分析检测 • 上一篇    下一篇

新化合物氟氧虫酰胺悬浮剂高效液相色谱方法的分析

周红霞1,华 春1,唐慧敏2   

  1. 1.南京晓庄学院生物化工与环境工程学院,江苏 南京 211171;2.江苏省农产品质量检验测试中心,江苏 南京 210036
  • 出版日期:2014-10-25 发布日期:2014-11-07
  • 基金资助:

    国家高技术研究发展计划(863计划)项目(2012AA021701)

Analysis of Novel Compound ZJ3757 Using High Performance Liquid Chromatography

ZHOU Hong-xia1, HUA Chun1, TANG Hui-min2   

  1. 1. School of Biochemical and Environmental Engineering, Nanjing Xiaozhuang University, Nanjing 211171, China;
    2. Jiangsu Agro-product Quality Test Center, Nanjing 210036, China
  • Online:2014-10-25 Published:2014-11-07

摘要:

建立新化合物氟氧虫酰胺的高效液相色谱分析方法,使用紫外检测器、C18液相色谱柱,以甲醇和水为流动相,在紫外检测波长250 nm条件下对其进行定性定量分析。结果表明,方法的相对标准偏差为0.27%,回收率在97.1%~105.6%之间,线性相关系数为0.999 8。

关键词: 氟氧虫酰胺, 高效液相色谱, 外标法

Abstract:

A high performance liquid chromatography (HPLC) method for the quantitative and qualitative analysis of
ZJ3757, an insecticide suspension, was established using a C18 column as the stationary phase, methanol and water as the
mobile phase, and UV detection at 250 nm. Results showed that the recovery of spiked samples was 97.1%–105.6% with
relative standard derivation (RSD) of 0.27%, and the linear correlation coefficient was 0.999 8.

Key words: ZJ3757, high performance liquid chromatography (HPLC), external standard method

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