食品科学 ›› 2011, Vol. 32 ›› Issue (24): 21-25.doi: 10.7506/spkx1002-6630-201124005

• 工艺技术 • 上一篇    下一篇

槟榔籽油提取工艺优化与脂肪酸成分分析

张伟敏1,魏静2,朱晓芳1,张海德1,*   

  1. 1. 海南大学食品学院 2. 海南省产品质量监督检验所
  • 出版日期:2011-12-25 发布日期:2011-12-29
  • 基金资助:
    “十一五”国家科技支撑计划项目(2007BAD76B03);海南大学科研基金项目(Rndy200501;hd09xm83)

Optimal Extraction and Fatty Acid Analysis of Seed Oil from Areca catechu L

ZHANG Wei-min1,WEI Jing2,ZHU Xiao-fang1,ZHANG Hai-de1,*   

  1. (1. College of Food Science, Hainan University, Haikou 570228, China; 2. Hainan Provincial Products Quality Supervision and Inspection Institute, Haikou 570203, China)
  • Online:2011-12-25 Published:2011-12-29

摘要: 目的:优化槟榔籽油的提取工艺,并分析槟榔籽油的成分。方法:采用传统溶剂法萃取槟榔籽油,对其工艺条件进行优化,并用气相色谱-质谱法(gas chromatography-mass spectrometry,GC-MS)对槟榔籽油所含的脂肪酸种类及含量进行测定。结果:槟榔籽油的最佳提取工艺条件为提取温度80℃、液料比24:1、提取时间11h,在此条件下油脂提取率可达12.84%。利用GC-MS鉴定出10个组分,占槟榔籽油脂肪酸总量的99.99%,主要含肉豆蔻酸(30.78%)、棕榈酸(19.23%)、油酸(26.86%)和亚油酸(19.56%)。结论:槟榔籽油中饱和脂肪酸达到51.18%,不饱和脂肪酸达到48.81%,其中多不饱和脂肪酸占总脂肪酸的20.10%。

关键词: 槟榔籽油, 提取工艺, GC-MS, 脂肪酸

Abstract: One-factor-at-a-time coupled with orthogonal array design method was employed to optimize the extraction of seed oil from Areca catechu by the traditional solvent method. The optimal extraction conditions were found to be: extraction at 80 ℃ for 11 h with n-hexane at a 24:1 ratio of material to liquid. Under these conditions, the extraction rate of seed oil from Areca catechu was 12.84%. Ten fatty acids were identified by GC-MS in the extracted oil, altogether accounting for 99.99% of the total fatty acids. The major fatty acids were myristic acid (30.78%), palmitic acid (19.23%), oleic acid (26.86%) and linoleic acid (19.56%). These results indicate that the seed oil contains 51.18% saturated fatty acids and 48.81% unsaturated fatty acids with a 20.10% relative content of polyunsaturated fatty acids in the total fatty acids.

Key words: seed oil from Areca catechu L, extraction process, gas chromatography-mass spectrometry (GC-MS), fatty acids

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