食品科学 ›› 0, Vol. ›› Issue (): 0-0.

• 基础研究 •    下一篇

热处理调控乳液凝胶微结构和不同维生素贮藏稳定性的研究

鹿瑶1,仇丹2,崔梦楠3,高彦祥4,5,毛立科4,5   

  1. 1. 中国农业大学食品学院
    2. 浙江大学;宁波工程学院
    3. 中国农业大学食品科学与营养工程学院
    4. 中国农业大学
    5. 中国农业大学
  • 收稿日期:2018-08-18 修回日期:2019-05-05 出版日期:2019-08-15 发布日期:2019-08-26
  • 通讯作者: 毛立科 E-mail:likemao@cau.edu.cn
  • 基金资助:
    国家自然科学基金

Study on the Effect of Thermal Treatment on the Microstructures of Emulsion Gels and Stability of Different Vitamins during Storage

  • Received:2018-08-18 Revised:2019-05-05 Online:2019-08-15 Published:2019-08-26
  • Supported by:
    National Natural Science Foundation

摘要: 本课题采用葡萄糖酸-δ-内酯诱导的方法制备乳清分离蛋白乳液凝胶,用于包埋亲水性功能因子异抗坏血酸钠和疏水性功能因子维生素E,研究乳液凝胶微结构与被包埋物质稳定性之间的关联机制。实验利用热处理(85℃)控制蛋白质的变性程度,并进而调控乳液凝胶的微结构和维生素的储藏稳定性。研究结果表明:随着蛋白质溶液热处理时间的延长,乳液油滴粒径增大、zeta-电位减小,而乳液的表观粘度无显著变化。质构和流变分析显示:热处理时间越长,凝胶的储能模量和硬度增加,但弹性降低。不同温度下的贮藏实验发现:蛋白质热处理时间的延长有利于提高乳液凝胶中复合维生素的稳定性,且复合功能因子之间存在协同作用。研究表明通过改变蛋白质热处理时间可以调控乳液凝胶的微结构,进而达到控制复合维生素贮藏稳定性的目的。

关键词: 乳液凝胶, 热处理, 微结构, 维生素, 稳定性

Abstract: Whey protein isolate (WPI) emulsion gels were prepared through glucono-δ-lactone (GDL) induced gelation, and the gels were used to simultaneously incorporate the hydrophilic and hydrophobic functional ingredients (sodium isoascorbate and vitamin E). The study focused on the relationship between the microstructures of emulsion gels and the stability of vitamins. Thermal treatment (85℃) was applied to modulate the denature level of protein, which then influenced the microstructures of the emulsion gels and stability of vitamins. The findings indicated that droplet size of the emulsion was increased, and zeta-potential was reduced with the increase in heating time, while the apparent viscosity was not significantly affected. Textural and rheological analysis showed that hardness and storage modulus of emulsion gels were enhanced with the increase in heating time, but the elasticity was weakened. Storage experiments at different temperatures revealed that the prolongation of heating time was beneficial to improve the stability of different vitamins, and there was a synergy effect between the mixed vitamins. It was concluded the microstructures of the emulsion gels could be adjusted by thermal treatment, which then can be used to control the stability different vitamins.

Key words: Emulsion gel, thermal treatment, microstructure, vitamins, stability

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