食品科学 ›› 2020, Vol. 41 ›› Issue (12): 228-233.doi: 10.7506/spkx1002-6630-20190508-071

• 成分分析 • 上一篇    下一篇

基于电子鼻与气相色谱-质谱联用区分不同陈酿期恒顺香醋风味物质

邝格灵,王新宇,李树,王昊,李信,余永建,赵国忠   

  1. (1.省部共建食品营养与安全国家重点实验室,天津科技大学食品工程与生物技术学院,天津 300457;2.江苏恒顺醋业股份有限公司,江苏 镇江 212143)
  • 出版日期:2020-06-25 发布日期:2020-06-22
  • 基金资助:
    天津科技大学大学生实验室创新基金项目(30003)

Discriminating the Volatile Flavor Composition of Hengshun Vinegars of Different Ages Using Electronic Nose and Gas Chromatography-Mass Spectrometry

KUANG Geling, WANG Xinyu, LI Shu, WANG Hao, LI Xin, YU Yongjian, ZHAO Guozhong   

  1. (1. State Key Laboratory of Food Nutrition and Safety, College of Food Engineering and Biotechnology, Tianjin University of Science and Technology, Tianjin 300457, China; 2. Jiangsu Hengshun Vinegar Ind. Co. Ltd., Zhenjiang 212143, China)
  • Online:2020-06-25 Published:2020-06-22

摘要: 为区分不同陈酿期恒顺香醋,并构建其香气特征,选取陈酿期3、5、10 a的恒顺香醋作为研究对象,采用电子鼻与气相色谱-质谱联用(gas chromatography-mass spectrometry,GC-MS)方法,并结合主成分分析和载荷分析量化主成分贡献率和样品间风味的区分度。结果显示:电子鼻能够很好地区分3 种不同陈酿期香醋的风味,电子鼻传感器W2S、W5S对恒顺香醋香气的区分能力最强。GC-MS分析结果表明糠醛和川芎嗪的相对含量对区别不同陈酿期恒顺香醋贡献率最大。可见,通过电子鼻技术和GC-MS相结合的手段,可以较好区分不同陈酿期的恒顺香醋,可为鉴别不同陈酿期的恒顺香醋提供理论依据和技术参考。

关键词: 恒顺香醋, 电子鼻, 气相色谱-质谱法, 风味

Abstract: In order to distinguish Hengshun vinegars of different ages and to establish their aroma characteristics, the volatile flavor compounds of 3-, 5-, and 10-year-old Hengshun vinegars were analyzed by gas chromatography-mass spectrometry (GC-MS) and their flavor characteristics were evaluated using an electronic nose. Principal component analysis (PCA) and loding analysis (LA) were performed to determine the contribution ratio of each principal component and the degree of differentiation among vinegars of different ages in terms of flavor. The results showd that the electronic nose could clearly discriminate the three vinegar samples with W2S and W5S being the most efficient sensors. In addition, GC-MS analysis showed that the relative contents of furfural and Ligustrazine contributed most to discriminate these vinegars. Therefore, our results support the combined use of electronic nose and GC-MS to discriminate Hengshun vinegars of different ages.

Key words: Hengshun balsamic vinegar, electronic nose, gas chromatography-mass spectrometry, flavor

中图分类号: