食品科学 ›› 2020, Vol. 41 ›› Issue (12): 243-249.doi: 10.7506/spkx1002-6630-20190723-302

• 工艺技术 • 上一篇    下一篇

石榴皮渣果胶电解水提取工艺及其结构特性

王炜清,庄虎,王康平,王萍,李述刚   

  1. (1.湖北工业大学生物工程与食品学院,菲利普斯亲水胶体研究中心,湖北 武汉 430068;2.塔里木大学生命科学学院,南疆特色农产品深加工兵团重点实验室,新疆 阿拉尔 843300)
  • 出版日期:2020-06-25 发布日期:2020-06-22
  • 基金资助:
    国家公益性行业(农业)科研专项(201503142-08)

Electrolyzed Water Extraction and Structural Characteristics of Pectin from Pomegranate Pomace

WANG Weiqing, ZHUANG Hu, WANG Kangping, WANG Ping, LI Shugang   

  1. (1. Glyn O. Phillips Hydrocolloid Research Centre, School of Food and Biological Engineering, Hubei University of Technology, Wuhan 430068, China; 2. Key Laboratory of South Xinjiang Special Agricultural Products Deep Processing Corps, College of Life Sciences, Tarim University, Alaer 843300, China)
  • Online:2020-06-25 Published:2020-06-22

摘要: 以石榴皮渣为研究对象,采用超声波辅助电解水法提取石榴皮渣果胶,优化石榴皮渣果胶的提取工艺,并分析其物质组成与结构特性。在单因素试验基础上,借助Box-Behnken试验设计优化,获得石榴皮渣果胶的最佳提取工艺条件:超声功率密度1 W/mL、pH 1.7、提取温度60 ℃、提取时间33 min和料液比1∶18(g/mL),石榴皮渣果胶提取得率达到14.95%。相比于超纯水提取工艺,其提取得率提高了2.2%,且电解水提取法得到的果胶具有更低的分子质量(7.294×106 g/mol)和更高的D-半乳糖醛酸质量分数(70.29%),并通过化学滴定法与傅里叶变换红外光谱手段共同说明了电解水提取法得到的果胶具有更高的酯化度。由此可知,超声辅助电解水提取法是一种高效、环保的提取方法,该结果为提高石榴果实产品附加值和实现副产物高效综合利用提供了技术支撑。

关键词: 石榴皮渣, 果胶, 电解水, 超声波

Abstract: In the paper, the ultrasonic-assisted electrolyzed water extraction of pectin from pomegranate (Punica granatum L.) pomace was optimized, and the composition and structural characteristics of the pectin were analyzed. Using combination of one-factor-at-a-time method and Box-Behnken design, the optimal extraction conditions were obtained as follows: ultrasonic power density, 1 W/mL; pH, 1.7; extraction temperature, 60 ℃; extraction time, 33 min; and material to liquid ratio, 1:18 (g/mL). Under these conditions, the pectin yield was 14.95%, which increased by 2.2% compared with the ultrapure water extraction process, and the pectin extracted with electrolyzed water (EWP) had a lower molecular mass (7.294 × 106 g/mol) and higher galacturonic acid content (70.29%). Analysis by combined use of the chemical titration method and Fourier transform infrared (FTIR) spectroscopy indicated that EWP had a higher degree of esterification. It can be seen that the ultrasonic-assisted electrolyzed water extraction method is an efficient and environmentally friendly method. This research provides technical support for producing value-added products from pomegranate fruit and realizing efficient and comprehensive utilization of by-products.

Key words: pomegranate pomace, pectin, electrolyzed water, ultrasound

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