食品科学 ›› 2010, Vol. 31 ›› Issue (24): 293-299.doi: 10.7506/spkx1002-6630-201024063

• 分析检测 • 上一篇    下一篇

4 种新疆单花蜜挥发性成分的SPME-GC-MS 分析

粟有志,谢丽琼,王强,阿不都拉·阿巴斯,李冠   

  1. 1.新疆大学生命科学与技术学院 2.新疆大学理化测试中心
  • 收稿日期:2010-02-24 出版日期:2010-12-25 发布日期:2010-12-29
  • 通讯作者: 李冠 E-mail:guanli@xju.edu.cn
  • 基金资助:

    新疆维吾尔自治区自然科学基金项目(200821102)

SPME-GC-MS Analysis of Volatile Compounds from Four XinJiang Monofloral Honey

SU You-zhi1,XIE Li-qiong1,WANG Qiang2,ABDULLA Abbas1,LI Guan1,*   

  1. 1. College of Life Science and Technology, Xinjiang University, Urumqi 830046, China;
    2. Physico-chemical Measurment Center, Xinjiang University, Urumqi 830046, China
  • Received:2010-02-24 Online:2010-12-25 Published:2010-12-29
  • Contact: LI Guan1 E-mail:guanli@xju.edu.cn

摘要:

采用固相微萃取(SPME)气质联用(GC-MS)分析新疆地区沙枣蜜、油菜蜜、葵花蜜以及棉花蜂蜜4 种单花蜜的挥发性成分。结果表明:39 份样品共检测出144 种挥发性成分;芳樟醇、2-(1,1- 二甲基)- 环己醇和联苯为沙枣蜜的特征性挥发组分;雪松醇为油菜蜜的特征性挥发物质;4- 萜品醇、9-(3,3- 二甲基- 环氧乙烷-2- 烷基)-2,7- 二甲基- 九碳-2,6- 二烯醇、2- 莰烯、1- 甲基-4- 异丙烯基苯、桃金娘烯醇、α,α,4- 三甲基-2,4- 环己二烯-1- 甲醇、α- 萜品醇为葵花蜜的特征性挥发物质,其中4- 萜品醇是葵花蜜最显著的特征性挥发物质;3- 苯基丙烯醛、3- 苯基-2- 丙烯醇为棉花蜜的特征性挥发组分。

关键词: 固相微萃取, 单花蜜, 挥发性成分, 气相色谱- 质谱联用

Abstract:

Volatile components in 4 kinds of monofloral hoeny from oleaster, sunflower, rape and cotton were analyzed by solid phase microextraction (SPME) followed by gas chromatography and mass spetrometry (GC-MS). A total of 144 volatile compounds were identified in 39 kinds of honey. Linalool, 2-(1,1-dimethylethyl)-cyclohexanol and diphene were the characteristic compounds in oleaster honey; cedrol was the characteristic compound in rape honey; 4-terpineol, 9-(3,3-dimethylepoxyethyl- 2-alkyl)-2,7-dimethyl-nona-2,6-enol, 2-camphene, 1-methyl-4-isopropenyl benzene, myrtenol, α,α,4-trimethyl- 2,4-cyclohexadiene-1-methanol andα-terpineol were the characteristic compounds in sunflower honey; 3-phenyl acrolein and 3-phenyl-2-allyl alcohol were the characteristic compounds in cotton honey.

Key words: solid-phase microextraction (SPME), monofloral honey, volatile compounds, gas chromatography and mass spetrometry (GC-MS)

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