Determination of 2-Naphthol in Fruits and Vegetables by High Performance Liquid Chromatography-Tandem Mass Spectrometry

doi:10.7506/spkx1002-6630-201312044

Abstract

Abstract:

An analytical method based on high performance liquid chromatography-tandem mass spectrometry was
developed for the determination of 2-naphthol in fruits and vegetables. Samples were extracted with acetonitrile, and the
extract was then cleaned up on an LC-NH2 cartridge. The analytes were determined by LC-MS/MS with electrospray
ionization source in multiple reaction monitoring (MRM). Quantification was conducted by external standard calibration.
Good linearity was observed in the range of 50.00 to 1000.00 μg/L (r2 ≥ 0.9997). The limit of detection of the established
method was 10 μg/kg. The recovery rate of 2-naphthol was 70.4%–105.5% at spiked levels of 10, 20 μg/kg and 50 μg/kg in
deferent samples, with relative standard deviation of 4.1%–10.6%.

Key words: high performance liquid chromatography-tandem mass spectrometry (LC-MS/MS), 2-naphthol, fruits, vegetables

XIA Shuang，XI Cun-xian，ZHANG Lei，YAN Ai-hua，TANG Bo-bin，WANG Guo-min，MU Zhao-de. Determination of 2-Naphthol in Fruits and Vegetables by High Performance Liquid Chromatography-Tandem Mass Spectrometry[J]. FOOD SCIENCE, doi: 10.7506/spkx1002-6630-201312044.

[1]	YANG Mengnan, LIU Shiqi, ZHANG Jing, RAN Longyi, CHEN Zhongjia, MA Chao. Isolation, Characterization and Application of Exosome-Like Nanoparticles from Fruits and Vegetables: A Review [J]. FOOD SCIENCE, 2021, 42(9): 355-361.
[2]	LI Kailong, CHEN Tongqiang, XU Wenyang, LI Tao, WANG Liangliang, WANG Fang, SUN Guifang. Ultrasonic Assisted Cloud Point Extraction Combined with Liquid Chromatography-Tandem Mass Spectrometry for the Determination of Natural Vitamin K Homologues in Vegetables [J]. FOOD SCIENCE, 2021, 42(8): 214-220.
[3]	WANG Mingshuang, JIANG Hanqian, LI Lin, ZHANG Liang, LIU Ruihai, LI Dongnan, LI Bin. Application of 3D Printing Technology in Foods Based on Fruits and Vegetables [J]. FOOD SCIENCE, 2021, 42(7): 345-351.
[4]	BAO Wei, HAN Jiaojiao, ZHANG Zhixuan, LU Chenyang, ZHOU Jun, MING Tinghong, LI Ye, SU Xiurong. Analysis of Microbial Community Diversity in Traditional Fermented Vegetables in Zhejiang Using High-throughput Sequencing [J]. FOOD SCIENCE, 2021, 42(6): 178-185.
[5]	GONG Lei, HUANG Hui, HAN Zhi, JIANG Feng, PENG Qingzhi, HUANG Zongqian, WANG Heng. Determination of 18 Succinate Dehydrogenase Inhibitor Fungicides in Foods by Modified QuEChERS Extraction Coupled with Ultra-high Performance Liquid Chromatography-Tandem Mass Spectrometry [J]. FOOD SCIENCE, 2021, 42(18): 261-268.
[6]	GAO Xia, CHEN Hui, TAN Min, LI Yuxiu, HE Honglin. Determination of Fipronil and Its Metabolites in Vegetables by Gas Chromatography-Negative Ion Chemical Ionization-Mass Spectrometry [J]. FOOD SCIENCE, 2021, 42(14): 333-338.
[7]	ZHOU Sainan, ZHANG Qing, WANG Fahe, WANG Xiaomei, LI Zhaojie, XUE Changhu, TANG Qingjuan. Optimization by Response Surface Methodology of the Formulation of Seaweeds, Fruits and Vegetables Extracts to Assist in Reducing Blood Glucose and Lipid Levels [J]. FOOD SCIENCE, 2021, 42(13): 57-63.
[8]	SHAO Ping, LIU Liming, WU Weina, CHEN Hangjun, GAO Haiyan. Research and Application of Sensors in Intelligent Packaging of Fruits and Vegetables [J]. FOOD SCIENCE, 2021, 42(11): 349-355.
[9]	YI Jianyong, ZHAO Yuanyuan, BI Jinfeng, Lü Jian, ZHOU Mo. A Review of Interactions between Cell Wall Polysaccharides and Polyphenols in Fruits and Vegetables [J]. FOOD SCIENCE, 2020, 41(9): 269-275.
[10]	LIANG Xiumei, ZHANG Weiyi, ZHANG Wei, XIE Shibing, HE Ruyi, XU Jing, SU Laijin, SUN Bolun, ZHANG Jing. Simultaneous Determination of Residues of 38 Pesticides in Fruits by QuEChERS Combined with High Performance Liquid Chromatography-Tandem Mass Spectrometry [J]. FOOD SCIENCE, 2020, 41(8): 288-296.
[11]	YANG Lüzhu, WANG Xinyu, WANG Rongrong, SHAN Yang, ZHANG Qun, DING Shenghua. Progress in the Knowledge of the Cuticle of Citrus Fruits and Its Effect on Postharvest Fruit Quality during Storage [J]. FOOD SCIENCE, 2020, 41(7): 234-244.
[12]	LIU Shasha, ZHANG Yuxiao, WANG Liang, YUN Liping, CHEN Yong, ZHANG Xinhua, GUO Yanyin. Effect of Active Modified Atmosphere on the Inhibition of Gilbertella persicaria [J]. FOOD SCIENCE, 2020, 41(5): 186-192.
[13]	XU Weili, FU Zhuang, WANG Xu, ZHAO Yue, WANG Chenzhao, MA Jiajun, WANG Zhibing. Homogeneous Liquid-Liquid Microextraction Based on the Solidification of Sedimentary Ionic Liquid Coupled with High Performance Liquid Chromatography for the Determination of Phenylurea Residues in Vegetables Samples [J]. FOOD SCIENCE, 2020, 41(4): 248-255.
[14]	CAO Xueqin, YANG Fei, CHEN Guotong, MAO Qiongling, LI Fang, YANG Zhong. Determination of 10 Preservative Residues in Fruits by Ultra-high Performance Liquid Chromatography-Tandem Mass Spectrometry [J]. FOOD SCIENCE, 2020, 41(4): 319-324.
[15]	YI Jianyong, MA Youchuan, BI Jinfeng, LI Xuan, WU Xinye, ZHOU Mo, FENG Shuhan. Bioavailability of Phenolic Compounds in Processed Fruits and Vegetables Products: A Review [J]. FOOD SCIENCE, 2020, 41(21): 351-358.

Determination of 2-Naphthol in Fruits and Vegetables by High Performance Liquid Chromatography-Tandem Mass Spectrometry

RichHTML

PDF (PC)

Knowledge

Abstract

Cite this article

share this article

References

Related Articles 15

Recommended Articles

Metrics

Comments