FOOD SCIENCE ›› 2019, Vol. 40 ›› Issue (24): 325-331.doi: 10.7506/spkx1002-6630-20181225-285

• Safety Detection • Previous Articles     Next Articles

Residues and Dissipation Dynamics of Abamectin and β-Cypermethrin in Pitaya (Hylocereus undatus) Fruit

LU Qiqi, TANG Mingxin, LIU Yushan, QU Liwen, SU Jiangli, ZHONG Guohua, LIU Jie   

  1. (Key Laboratory of Crop Integrated Pest Management in South China, Ministry of Agriculture, College of Agriculture, South China Agricultural University, Guangzhou 510642, China)
  • Online:2019-12-25 Published:2019-12-24

Abstract: In order to examine the residual levels and dissipation dynamics of abamectin and β-cypermethrin (β-CP) in pitaya fruit, the fruit were sprayed with 5.2% abamectin-β-CP emulsifiable concentrate (EC) at a recommended dose of 46.8 g/hm2 at different times before harvest. The two insecticides were extracted from the fruit samples using acetone, purified and then concentrated prior to analysis. Abamectin was detected by reversed-phase high performance liquid chromatography while β-CP by gas chromatography. The limits of detection (LODs) were 0.002 and 0.02 ng/μL, and the limits of quantification (LOQs) 0.005 and 0.1 mg/kg for abamectin and β-CP, respectively. The spiked recoveries ranged from 93.8% to 97.2% for abamectin and from 94.0% to 99.2% for β-CP with relative standard deviations (RSDs) less than 9.4%. The dissipation dynamics of abamectin and β-CP sprayed on pitaya fruit was fitted to a first-order kinetic model, and their half-lives were 2.76–4.20 and 3.09–6.08 d, respectively. The final minimum residue values of abamectin and β-CP were < 0.005 and < 0.1 mg/kg, respectively, and the maximum residue values 0.009 and 0.13 mg/kg, respectively. The results showed that the abamectin-β-CP EC could be fast degraded and the pre-harvest interval (PHI) was 14 d, so that it could be recommended for safe pest management. The present study provides basic data and a useful guidance for the use and safety evaluation of abamectin and β-CP on tropical fruits.

Key words: abamectin, β-cypermethri, Hylocereus undatus, residue, dissipation dynamics

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