食品科学

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芭蕉芋支链淀粉的结构表征与流变学特性分析

石海信,李 桥,陆来仙,顾 静   

  1. 钦州学院化学化工学院,广西 钦州 535000
  • 出版日期:2013-10-15 发布日期:2013-09-27
  • 通讯作者: 石海信
  • 基金资助:

    广西自然科学基金项目(2013GXNSFAA019023);广西高校科学技术研究项目(2013YB257)

Structure Characterization and Rheological Properties of Edible Canna (Canna edulis Ker.) Amylopectin

SHI Hai-xin,LI Qiao,LU Lai-xian,GU Jing   

  1. College of Chemistry and Chemical Engineering, Qinzhou University, Qinzhou 535000, China
  • Online:2013-10-15 Published:2013-09-27
  • Contact: SHI Hai-xin

摘要:

利用扫描电子显微镜(SEM)和红外光谱仪(FTIR)对芭蕉芋支链淀粉(CAP)的颗粒形貌及结构进行表征,并利用乌氏黏度计和数显黏度计对CAP的流变学特性进行研究。SEM结果表明:CAP大部分颗粒黏连在一起成团粒状,部分区域出现孔洞。FT-IR分析显示:CAP仍具有芭蕉芋原淀粉的基本化学基团,但无序化程度增加。流变性能研究表明:CAP的特性黏度为43.6mL/g;CAP糊液呈假塑性流体特征,用幂率定律能较好地对CAP糊液的流变曲线进行拟合。

关键词: 芭蕉芋淀粉, 支链淀粉, 正丁醇-异戊醇重结晶法, 结构表征, 流变行为

Abstract:

The structure and morphology of edible canna amylopectin (CAP) were characterized by scanning electron
microscopy (SEM) and Fourier transform infrared spectroscopy (FTIR) and its rheological properties were studied using
Ubbelohde viscometer and digital display viscometer. SEM results indicated that most CAP granules were bound together
into pellets, and some holes are observed. FTIR analysis showed that the chemical groups of CAP were identical to those
of edible canna starch, despite showing an increased degree of disorder. Moreover, the intrinsic viscosity of CAP was
43.6 mL/g, CAP paste behaved as a pseudoplastic fluid, and the rheological curve of CAP could be well fitted by the
power rate law.

Key words: edible canna starch, amylopectin, n-butanol-isoamyl alcohol recrystallization, structure characterization, rheological behavior

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