食品科学 ›› 2024, Vol. 45 ›› Issue (22): 173-179.doi: 10.7506/spkx1002-6630-20231219-153

• 成分分析 • 上一篇    下一篇

基于气相色谱-质谱法和电子鼻技术分析不同烘烤度荔枝木对荔枝白兰地陈酿风味的影响

黄晨, 曹慧颖, 郭德军,, 王润铃   

  1. (1.北部湾大学食品工程学院,广西 钦州 535011;2.广西大学轻工与食品工程学院,广西 南宁 530004;3.钦州市特色果蔬发酵重点实验室,广西 钦州 535011)
  • 出版日期:2024-11-25 发布日期:2024-11-05
  • 基金资助:
    钦州市科技攻关项目(202014820)

Effects of Different Toasting Degrees of Lychee Wood on the Flavor of Lychee Brandy Analyzed by Electronic Nose and Gas Chromatography-Mass Spectrometry

HUANG Chen, CAO Huiying, GUO Dejun,, WANG Runling   

  1. (1. College of Food Engineering, Beibu Gulf University, Qinzhou 535011, China; 2. College of Light Industry and Food Engineering, Guangxi University, Nanning 530004, China; 3. Qinzhou Key Laboratory of Fruit and Vegetable Fermentation, Qinzhou 535011, China)
  • Online:2024-11-25 Published:2024-11-05

摘要: 为研究不同烘烤程度荔枝木片对荔枝白兰地陈酿风味的影响,在荔枝白兰地原酒中分别加入不同烘烤程度荔枝木片进行陈酿,以原酒和添加重度烘烤橡木片陈酿的荔枝白兰地作对照,运用感官评价、电子鼻和气相色谱-质谱联用仪对5 种不同陈酿的荔枝白兰地品质、挥发性风味成分进行评定和分析。结果表明,电子鼻分析结果与感官评定结果具有较好的一致性,添加重度烘烤荔枝木片陈酿的荔枝白兰地感官综合评分最高;5 种酒样中共检测出44 种挥发性香气化合物,5 种荔枝白兰地酒样中挥发性成分的种类和含量差异较大,同时都具有独特的烯烃类风味物质;陈酿荔枝白兰地的主要的成分为醇类、酯类、烯烃类,而醛酮、烷烃和芳香烃类物质的含量和种类相对较少;癸酸乙酯、乙酸乙酯、辛酸乙酯、2-甲基丁醇、异戊醇、异丁醇、α-石竹烯和β-石竹烯共同构成了陈酿荔枝白兰地的主要风味成分特征。与加入重度烘烤橡木片陈酿的荔枝白兰地相比,原酒中添加适量的重度烘烤荔枝木片更有利于其品质的提升。

关键词: 荔枝白兰地;荔枝木;烘烤度;气相色谱-质谱法;电子鼻

Abstract: In order to study the effects of lychee wood chips with different toasting degrees used in the aging process on the flavor of lychee brandy, the quality and volatile flavor components of lychee brandy aged with lightly toasted (LT), moderately toasted (MT) or heavily toasted (HT) lychee wood chips were evaluated and analyzed using sensory evaluation, electronic nose and gas chromatography-mass spectrometry. Raw and aged lychee brandy with heavily toasted oak chips were used as controls. The results of electronic nose analysis were in good agreement with those of sensory evaluation, and the brandy aged with heavily roasted lychee wood chip wood had the highest overall sensory score. A total of 44 volatile aroma compounds were identified in the five brandy samples, and the types and contents of volatile components varied greatly among these samples, each with their unique olefinic flavor substances. The major volatile components of aged lychee brandy were alcohols, esters, olefins, along with lesser amounts of aldehydes and ketones, alkanes, and aromatic hydrocarbons. Ethyl decanoate, ethyl acetate, ethyl caprylate, 2-methylbutanol, isoamyl alcohol, isobutanol, alpha stigmasterol and beta stigmasterol together constituted the major flavor profile of the aged lychee brandy. Therefore, aging with a moderate amount of heavily roasted lychee wood chips resulted in better improvement in the quality of lychee brandy compared to heavily toasted oak chips.

Key words: lychee brandy; lychee wood; toasting degree; gas chromatography-mass spectrometry; electronic nose

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