Determination of O-Phenlyphenol in Orange Peel by Solvent Extraction Coupled with Differential Pulse Stripping Voltammetry

doi:10.7506/spkx1002-6630-201106045

FOOD SCIENCE ›› 2011, Vol. 32 ›› Issue (6 ): 195-197.doi: 10.7506/spkx1002-6630-201106045

• Analysis & Detection • Previous Articles Next Articles

Determination of O-Phenlyphenol in Orange Peel by Solvent Extraction Coupled with Differential Pulse Stripping Voltammetry

LI Jing1，LI Hong-bo1,2,*，DU Shi2，REN Yan-yan2，HU Xiao-ya2

1. College of Chemical and Biological Engineering, Yancheng Institute of Technology, Yancheng 224051, China；
2. College of Chemistry and Chemical Engineering, Yangzhou University, Yangzhou 225002, China

Received:2010-06-18 Revised:2011-01-24 Online:2011-03-25 Published:2011-03-03
Contact: LI Hong-bo E-mail:lhbchem@163.com

Abstract

Abstract: The solvent extraction-differential pulse stripping voltammetry method was developed to determine O-phenlyphenol (OPP) in orange peel. In order to avoid the influence of ascorbic acid and essential oil, OPP was extracted by toluene from orange peel. Under the optimal conditions, differential pulse stripping voltammetry was used to determine OPP in orange peel. The results demonstrated that the oxidative peak current of OPP was linearly correlated with the OPP concentrations in the range of 2.0 × 10-9 －4.0 × 10-6 mol/L. The detection limit and recovery rate of this developed method were 8.1 × 10-10 mol/L and 106.7%－112.2%, respectively. Therefore, this developed method is characteristics of simple operation, fast detection, high sensitivity and accuracy.

Key words: electrochemistry, solvent extraction, O-phenlyphenol, orange peel

CLC Number:

O657. 1

LI Jing1，LI Hong-bo1,2,*，DU Shi2，REN Yan-yan2，HU Xiao-ya2. Determination of O-Phenlyphenol in Orange Peel by Solvent Extraction Coupled with Differential Pulse Stripping Voltammetry[J]. FOOD SCIENCE, 2011, 32(6 ): 195-197.

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Determination of O-Phenlyphenol in Orange Peel by Solvent Extraction Coupled with Differential Pulse Stripping Voltammetry

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