食品科学 ›› 2011, Vol. 32 ›› Issue (8): 197-201.doi: 10.7506/spkx1002-6630-201108045

• 分析检测 • 上一篇    下一篇

蒸馏萃取-气相色谱-质谱联用对不同腌制工艺大头菜挥发性风味物质的分析

曾凡坤 王金美   

  1. 西南大学食品科学学院
  • 出版日期:2011-04-25 发布日期:2011-04-12
  • 基金资助:
    国家星火计划项目(2007EA811032)

Effect of Pickling Process on Volatile Flavor compounds in Pickled Mustard Root as Analyzed by SDE/GC-MS

ZENG Fan-kun,WANG Jin-mei   

  1. College of Food Science, Southwest University, Chongqing 400715, China
  • Online:2011-04-25 Published:2011-04-12

摘要: 采用同时蒸馏萃取-气相色谱-质谱联用(SDE-GC-MS)对不同加工工艺大头菜和原料的挥发性风味物质进行分析。从大头菜原料、新工艺大头菜、传统腌制大头菜、脱盐大头菜4个样品中共检验出90种挥发性香气物质,其中从新工艺大头菜、传统腌制大头菜和脱盐大头菜中分别检测出68、56和28种挥发性香气物质;大头菜腌制可产生大量挥发性风味成分,且新工艺大头菜挥发性香气成分种类高于传统大头菜和脱盐大头菜,脱盐导致大头菜香气成分大量损失。

关键词: 大头菜, 腌制, 挥发性风味物质, 气相色谱/质谱联用

Abstract: Simultaneous distillation extraction (SDE) followed by GC-MS was used to investigate the volatile flavor composition of pickled mustard root samples from different processing methods. A total of 90 volatile compounds were identified in 4 samples, including raw mustard root, traditional pickled mustard root and its desalted counterpart and mustard root pickled by a novel process, of which 68, 56 and 28 were present in novel pickled mustard root as well as traditional pickled mustard root and its desalted counterpart, respectively. Overall, pickling process results in the formation of many new volatiles. However, more are formed by the new process compared with the other two. Meanwhile, desalting process may result in a substantial loss of volatile compounds.

Key words: mustard root, pickling, volatiles, gas chromatography-mass spectrometry (GC-MS)

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