食品科学 ›› 2024, Vol. 45 ›› Issue (5): 118-125.doi: 10.7506/spkx1002-6630-20230828-196

• 成分分析 • 上一篇    下一篇

基于气相色谱-离子迁移谱分析不同产地秋月梨品质差异

何婉琳,施露,林梦桦,李亚辉,梁颖,张志勇   

  1. (1.江苏大学食品与生物工程学院,江苏 镇江 212013;2.江苏省食品质量安全重点实验室,江苏省农业科学院农产品质量安全与营养研究所,江苏 南京 210014)
  • 出版日期:2024-03-15 发布日期:2024-04-03
  • 基金资助:
    现代农业产业技术体系建设专项(CARS-28);江苏省农业科技自主创新资金项目(cx(23)3050)

Quality Analysis of ‘Akizuki’ Pear Fruit (Pyrus pyrifolia) from Different Geographical Origins by Gas Chromatography-Ion Mobility Spectrometry

HE Wanlin, SHI Lu, LIN Menghua, LI Yahui, LIANG Ying, ZHANG Zhiyong   

  1. (1. School of Food and Biological Engineering, Jiangsu University, Zhenjiang 212013, China; 2. Key Laboratory of Food Quality and Safety of Jiangsu Province, Institute of Food Safety and Nutrition, Jiangsu Academy of Agricultural Sciences, Nanjing 210014, China)
  • Online:2024-03-15 Published:2024-04-03

摘要: 为探究不同产地秋月梨品质特征,对6 个产地秋月梨果实品质指标进行测定,并利用气相色谱-离子迁移谱(gas chromatography-ion mobility spectrometry,GC-IMS)测定其挥发性香气成分。结果显示,河南宁陵县秋月梨可滴定酸含量显著高于其他产地,部分产地秋月梨之间可溶性固形物含量、总黄酮与总酚存在显著差异(P<0.05)。6 个产地秋月梨梨皮和梨肉中共鉴定出76 种挥发性香气成分,其中酯类23 种、醛类20 种、醇类11 种、酮类4 种、烯烃类1 种、酸类3 种、其他类14 种,梨皮中挥发性香气成分比梨肉中多24 种。河北魏县检出特有挥发性香气成分乙酸异丁酯、丁酸甲酯和异戊醛。通过指纹图谱和相似度分析较好实现了不同产地秋月梨区分。该研究提供了不同产地秋月梨品质和挥发性香气信息,GC-IMS技术具有实现秋月梨产地区分和产地溯源的潜在应用前景。

关键词: 秋月梨;气相色谱-离子迁移谱;挥发性香气成分;产地;指纹图谱

Abstract: In order to explore the quality characteristics of ‘Akizuki’ pear fruit (Pyrus pyrifolia) from different regions, the quality indexes of pear fruit from six geographical origins were determined, and gas chromatography-ion mobility spectrometry (GC-IMS) was used to determine their volatile aromatic compounds. The results showed that the titratable acid content of pear fruit from Ningling, Henan province was significantly higher than that of pear fruit from the other regions. There were significant differences in the contents of soluble solids, total flavonoids, and total phenols among some regions (P < 0.05). Totally 76 volatile aroma components were identified in the pericarp and pulp of pear fruit from the six different regions, including 23 esters, 20 aldehydes, 11 alcohols, 4 ketones, 1 olefin, 3 acids, and 14 other compounds. There were 24 more volatile aroma components in the pericarp than in the pulp. The unique volatile aroma components including isobutyl acetate, methyl butyrate, and isovaleraldehyde were detected in pear fruit from Weixian, Hebei province when compared with the other regions. Similarity analysis from fingerprints showed clear distinction among pear fruit from different regions. This study has provided information about the quality and aroma characteristics of ‘Akizuki’ pear fruit from different regions, and demonstrated that GC-IMS has potential application prospects for geographical origin differentiation and traceability of ‘Akizuki’ pear fruit.

Key words: ‘Akizuki’ pear fruit; gas chromatography-ion mobility spectrometry; volatile components; production regions; fingerprints

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