食品科学 ›› 2025, Vol. 46 ›› Issue (11): 302-309.doi: 10.7506/spkx1002-6630-20241209-062

• 包装贮运 • 上一篇    

基于挥发性盐基氮的动力学模型预测板鸭干货架期

但利,何丽,刁尚鹏,邢亚阁,许青莲,刘洪,吕兴禹,叶杨阳,洛果巫惹莫   

  1. (1.西华大学食品与生物工程学院,四川 成都 610039;2.德昌县茂源长(童耳朵)食品有限责任公司,四川 凉山 615599)
  • 发布日期:2025-05-14
  • 基金资助:
    四川省区域创新合作项目(2024YFHZ0207)

Kinetic Modeling for Shelf-Life Prediction of Dry Salted Duck Based on Total Volatile Basic Nitrogen

DAN Li, HE Li, DIAO Shangpeng, XING Yage, XU Qinglian, LIU Hong, LÜ Xingyu, YE Yangyang, WUREMO Luoguo   

  1. (1. School of Food and Bioengineering, Xihua University, Chengdu 610039, China;2. Dechang County Maoyuanchang (Tong Ear) Food Co. Ltd., Liangshan 615599, China)
  • Published:2025-05-14

摘要: 以大凉山手撕板鸭干为对象,建立不同贮藏温度条件下大凉山手撕板鸭干货架期预测模型。分析大凉山手撕板鸭干在不同贮藏温度(25、30、37 ℃)条件下感官评分、挥发性盐基氮(total volatile basic nitrogen,TVB-N)、过氧化值(peroxide value,POV)、硫代巴比妥酸(thiobarbituric acid,TBA)、a*值等指标的变化及相关性,采用化学反应动力学方程和Arrhenius方程分析构建手撕板鸭干的货架期预测模型并进行货架期预测。结果表明,不同贮藏温度条件下手撕板鸭干的感官评分、a*、aw、pH值随贮藏时间的延长而逐渐降低;TVB-N、POV、TBA值均随着贮藏时间的延长而逐渐上升,且变化趋势为37 ℃>30 ℃>25 ℃;通过分析不同贮藏温度条件下手撕板鸭干的感官指标与各理化指标之间的Pearson相关系数,推断TVB-N可作为预测手撕板鸭干货架期的有效指标。通过TVB-N的货架期预测模型,推断出手撕板鸭干在25、30、37 ℃贮藏温度条件下的货架期可能为305、255、204 d。在贮藏前100 d内,该模型的预测值与实测值的相对偏差在10%以内,证明该模型准确可信,能够快速可靠地预测板鸭干的货架期。

关键词: 大凉山板鸭干;贮藏温度;品质;货架期预测模型

Abstract: A model for predicting the shelf-life of Daliangshan hand-torn duck at different storage temperatures was established. Changes in the sensory score, total volatile basic nitrogen (TVB-N), peroxide value (POV), thiobarbituric acid (TBA) value, and a* value of dry salted duck stored at 25, 30 or 37 ℃ were analyzed and the correlation among them was examined. Chemical reaction kinetic equations and the Arrhenius equation were used to develop a shelf-life prediction model for hand-torn dried duck. The results showed that the sensory score, a*, water activity (aw) and pH decreased with storage time, irrespective of storage temperature, while the opposite trend was observed for the TVB-N, POV and TBA value. The changing trend was 37 ℃ > 30 ℃ > 25 ℃. Pearson’s correlation coefficients between the sensory attributes and the physicochemical indexes showed TVB-N to be an effective quality index to predict the shelf-life of hand-torn dried duck. According to the proposed prediction model, the estimated shelf-life of dry salted duck was 305, 255 and 204 d at 25, 30 and 37 ℃, respectively. Within the first 100 days of storage, the relative deviation between the predicted value and the measured value was less than 10%, demonstrating high accuracy and reliability of the model. In conclusion, this model could allow quick and reliable prediction of the shelf-life of dry salted duck.

Key words: Daliangshan dry salted duck; storage temperature; quality; shelf life prediction model

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