食品科学 ›› 2007, Vol. 28 ›› Issue (1): 285-288.

• 分析检测 • 上一篇    下一篇

白丁香鲜花挥发性化学成分研究

 吕金顺, 朱惠琴, 周建峰, 朱巧军   

  1. 江苏省低维材料化学重点建设实验室 淮阴师范学院; 江苏省低维材料化学重点建设实验室; 淮阴师范学院; 甘肃中医学院基础部; 江苏淮安223001; 甘肃兰州731000;
  • 出版日期:2007-01-15 发布日期:2011-12-31

Study on Flower Volatile Chemical Compositions from Syringa oblata var.affinis Lingelsh.

 吕Jin-Shun , ZHU  Hui-Qin, ZHOU  Jian-Feng, ZHU  Qiao-Jun   

  1. 1.Jiangsu Key Laboratory for Chemistry of Low-Dimensional Materials,Huaiyin Teachers College, Huai’an 223001, China; 2.Gansu College of TCM, Lanzhou 731000, China
  • Online:2007-01-15 Published:2011-12-31

摘要: 用水蒸汽蒸馏法提取和GC-MS联用仪检测了白丁香鲜花的挥发性成分,并用已有的文献作了比较。发现采用不同方法对白丁香鲜花提取测试的挥发性成分有所不同。直接吸附法得到的化合物有27种,主要是为萜烯、金合欢烯类、桉树脑、丁香醛及其醇的系列化合物,是香料的头香和昆虫信息素的特征化合物,水蒸汽蒸馏法得到的化合物有46种,包括上述部分化合物和主要的香料和药物特征组分:苯乙醇、丁香醛系列化合物、(Z)-3-己烯-1-醇、2-甲氧基-4-乙烯基苯酚、金合欢醇、9-十九烯等烯类、烷烃类等化合物。两种方法结合是准确确定鲜花低挥发性成分作为香料的头香及其他香、昆虫信息素和抗菌抗炎药物的研究方法。

关键词: 白丁香鲜花, 挥发性成分, GC-MS, 昆虫信息素, 香料, 药物

Abstract: The chromatography-mass spectrometer (GC-MS) techniques,compared with published literatures were employed to study the volatile constituents of Syringa oblate var.affinis Lingelsh. flower by steam distillation and direct adsorption. The results indicated that volatile constituents are different with different extracting methods. 27 compounds, obtained by the direct adsorption and 45 compounds, obtained by the steam distillation, are identified by GC-MS technique from the flower. The principle compounds by direct adsoption, the characteristic headspace volatile compounds of perfume and insect pheromone, are terpene, lilac aldehyde A-D, lilac alcohol A-D, farnesene ect by direct adsorption. And the other compounds by steam distillation, the characteristic compounds of other perfume and medicament, are terpene, phenylethyl alcohol, lilac aldehyde A- D,3 -hexen-1-ol,(Z),2 -methoxy-4-vinylphenol,2 ,6,10-dodecatrien-1-ol, 3,7,11-trimethyl-,9 -Nonadecene, alkane ect.Byc ombining direct adsorption with steam distillation,it is a good and correct method for determining low volatile constituents of fresh flowers, used for headspace volatile perfume or other kind of perfume, insect pheromone and medicament.

Key words: flower of Syringa oblate var.affinis, constituent of volatile oil, GC-MS, insect pheromone, perfume, medicament