食品科学 ›› 2009, Vol. 30 ›› Issue (24 ): 393-396.doi: 10.7506/spkx1002-6630-200924089

• 分析检测 • 上一篇    下一篇

花生酱挥发性风味成分的鉴定

楼 飞1,刘 源1,孙晓红1,潘迎捷1,赵俊红2,赵 勇1 ,*   

  1. 1.上海海洋大学食品学院 2.上海市食品研究所
  • 收稿日期:2009-08-31 出版日期:2009-12-15 发布日期:2010-12-29
  • 通讯作者: 赵 勇1 ,* E-mail:yzhao@shou.edu.cn
  • 基金资助:

    上海市青年科技启明星计划资助项目(07QA14047);上海市科委重大科技攻关项目(07DZ19508);国家“863”计划项目(2008AA100804);国家自然科学基金项目(30901125)

Identification of Volatile Flavor Components in Peanut Butter

LOU Fei1,LIU Yuan1,SUN Xiao-hong1,PAN Ying-jie1,ZHAO Jun-hong2,ZHAO Yong1,*   

  1. LOU Fei1,LIU Yuan1,SUN Xiao-hong1,PAN Ying-jie1,ZHAO Jun-hong2,ZHAO Yong1,*
  • Received:2009-08-31 Online:2009-12-15 Published:2010-12-29
  • Contact: ZHAO Yong1,* E-mail:yzhao@shou.edu.cn

摘要:

采用电子鼻法对两种知名品牌花生酱A 和B 中的挥发性风味物质进行主成分分析。采用顶空固相微萃取方法提取花生酱A和B中的挥发性风味物质,结合气相色谱- 质谱联用技术对提取的挥发性风味物质进行分离鉴定。电子鼻法能很好的区分花生酱A 和B。从花生酱A 中共鉴定出62 种化合物,占总检出化合物的94.68%,吡嗪类化合物含量最高,有19 种,占总挥发性成分的51.86%;花生酱B 中共鉴定出42 种化合物,占总检出化合物的90.98%,吡嗪类化合物含量最高,有13 种,占总挥发性成分的44.40%。两种花生酱中含有39 种相同的挥发性风味物质,主要是吡嗪、醛类、呋喃、吡咯、酮类、醇类等化合物,相对百分含量有差别。本研究表明,花生酱主要的挥发性化合物是吡嗪类化合物,而且电子鼻结合顶空固相微萃取以及气- 质联用技术可以对不同品牌花生酱的风味进行很好区分。

关键词: 花生酱, 电子鼻, 顶空固相微萃取法, 气相色谱- 质谱法, 挥发性成分

Abstract:

Electronic nose (E-nose) was employed to analyze volatile flavor compounds in peanut butter from two different brands through principal component analysis (PCA) method. Headspace solid phase micro-extraction (SPME) technique was used to extract volatile flavor compounds from peanut butter A and B. Volatile flavor components in peanut butter were isolated and identified by capillary gas chromatography mass spectrometry (GC-MS). Electronic nose could successfully identify peanut butter A and B. Totally 62 and 42 volatile flavor components were identified and their contents were 94.68% and 90.98% among total determined components from peanut butter A and B, respectively. Pyrazines exhibited the highest content in both kinds of peanut butter. The contents of 19 and 13 pyrazines were 51.86% and 44.40% in total volatile components from both kinds of peanut butter, respectively. Meanwhile, 39 volatile flavor components such as pyrazines, aldehydes, furan, pyrrole, ketones and alcohols were identified to be same in both peanut butter A and B, although their contents are different. This investigation confirmed that major flavor compounds in peanut butter were pyrazines. E-nose combined with GC-MS and SPME technology provided an excellent identification method for aromatic components from different brands of peanut butter.

Key words: peanut butter, electronic nose, headspace solid-phase microextraction, gas chromatography-mass spectrometry, volatile flavor compounds

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