食品科学 ›› 2020, Vol. 41 ›› Issue (20): 205-210.doi: 10.7506/spkx1002-6630-20190516-177

• 成分分析 • 上一篇    下一篇

基于SPME-GC-MS探讨盐渍处理对苦水玫瑰纯露挥发性成分构成的影响

武艺,胡建忠,韩雪,殷丽强,袁玮琼,施昊,吕兆林   

  1. (1.北京林业大学生物科学与技术学院,北京 100083;2.水利部水土保持植物开发管理中心,北京 100037;3.兰州九香玫瑰生物科技有限公司,甘肃 兰州 730000;4.北京林业大学公共分析测试中心,北京 100083;5.林业食品加工与安全北京市重点实验室,北京 100083)
  • 出版日期:2020-10-25 发布日期:2020-10-23
  • 基金资助:
    水利部水土保持植物开发管理中心项目(2019HXFWSWXY006)

Effects of Salt Treatment on Volatile Components of Kushui Rose (Rosa setate × R. rugosa) Hydrosol Analyzed by SPME-GC-MS

WU Yi, HU Jianzhong, HAN Xue, YIN Liqiang, YUAN Weiqiong, SHI Hao, LÜ Zhaolin   

  1. (1. College of Biological Sciences and Technology, Beijing Forestry University, Beijing 100083, China;2. Development and Management Center of Soil and Water Conservation Plants, Ministry of Water Resources, Beijing 100037, China;3. Lanzhou Jiuxiang Rose Biotechnology Co. Ltd., Lanzhou 730000, China;4. Analysis and Testing Center, Beijing Forestry University, Beijing 100083, China;5. Beijing Key Laboratory of Forestry Food Processing and Safety, Beijing 100083, China)
  • Online:2020-10-25 Published:2020-10-23

摘要: 研究不同盐渍条件下苦水玫瑰纯露的挥发性成分差异,揭示盐渍处理对玫瑰纯露挥发性成分构成的影响。以苦水玫瑰为材料,采用自主研发装置制备纯露,并用固相微萃取-气相色谱-质谱联用技术对其挥发性成分进行分析。研究表明:未经NaCl盐渍的苦水玫瑰鲜花和经NaCl盐渍的苦水玫瑰制备得到的纯露,共鉴定出86 种化合物,鲜花纯露中鉴定出57 种化合物,主要以香茅醇和芳樟醇为主,盐渍纯露中鉴定出61 种化合物,主要为香茅醇、芳樟醇和松油醇。与鲜花纯露相比,盐渍纯露中芳樟醇和松油醇相对含量显著增加(P<0.05),香茅醇相对含量显著降低(P<0.05);两种纯露中的酚类物质相对含量相近(P>0.05),分别为3.84%和3.81%。鲜花纯露中还有10 种醛酮类物质(0.42%)、3 种烯类物质(0.21%)等,盐渍纯露中有11 种醛酮类物质(0.69%)、1 种烯类物质(0.17%)。两种纯露在成分构成上虽均以醇类物质为主,但其种类、数量和相对含量各不相同,同时,鲜花纯露的香气比盐渍纯露更饱满香甜,颜色更澄清。本研究为玫瑰纯露的制备及品质鉴定提供一定的理论支撑。

关键词: 苦水玫瑰纯露;盐渍条件;品质;固相微萃取-气相色谱-质谱联用技术;挥发性成分

Abstract: The difference in the volatile composition of Kushui rose hydrosol under different salt treatment conditions was studied in an attempt to reveal the influence of salt treatment on the quality of rose hydrosol. In this experiment, Kushui rose hydrosol was prepared from the flowers of Rosa setate × R. rugosa using a device developed by ourselves, and its volatile components were analyzed by solid phase microextraction-gas chromatography-mass spectrometry (SPME-GC-MS). The study results showed that a total of 86 volatile compounds were identified from the hydrosols of fresh and NaCl treated flowers, 57 volatile compounds of which were present in the fresh hydrosol mainly citronellol and linalool, and 61 volatile compounds in the salted hydrosol mainly citronellol, linalool and terpineol. Compared with the fresh one, the contents of linalool and terpineol in the salted hydrosol were significantly increased (P < 0.05), while the content of citronellol was significantly decreased (P < 0.05). The contents of phenolic compounds in the two hydrosols were similar (P > 0.05), which were 3.84% and 3.81%, respectively; there were also 10 aldoketones (0.42%) and 3 terpenes (0.21%) in the fresh hydrosol. Additionally, there were 11 aldoketones (0.69%) and 1 terpene (0.17%) in the salted hydrosol. Although the two types of hydrosols were mainly composed of alcohols, the types, quantities and relative percentages of alcohols were quite different between them. At the same time, the aroma of the fresh hydrosols was more abundant and sweeter than the salted one, and the color was clearer. This study provides theoretical support for the preparation and quality identification of rose hydrosols.

Key words: Kushui rose hydrosols; salt treatment conditions; quality; solid phase microextraction-gas chromatography-mass spectrometry; volatile compounds

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