食品科学 ›› 2022, Vol. 43 ›› Issue (10): 271-280.doi: 10.7506/spkx1002-6630-20210514-164

• 成分分析 • 上一篇    下一篇

甜玉米成熟过程中挥发性风味物质的变化规律

李国琰,张雁,廖娜,邓媛元,王智明,李巧玲,王蒙,黄成宜   

  1. (1.广东省农业科学院蚕业与农产品加工研究所,农业农村部功能食品重点实验室,广东省农产品加工重点实验室,广东 广州 510610;2.河北科技大学食品与生物学院,河北 石家庄 050018;3.广东天之源农业科技有限公司,广东 江门 529100)
  • 出版日期:2022-05-25 发布日期:2022-05-27
  • 基金资助:
    广东省现代农业产技术体系创新团队项目(2020KJ135);广东省本土创新创业团队项目(2019BT02N112); 广东省农业科学院农业优势产业学科团队建设项目(202108TD)

Changes of Volatile Flavor Compounds in Sweet Corn during Maturation

LI Guoyan, ZHANG Yan, LIAO Na, DENG Yuanyuan, WANG Zhiming, LI Qiaoling, WANG Meng, HUANG Chengyi   

  1. (1. Key Laboratory of Functional Foods, Ministry of Agriculture and Rural Affairs, Guangdong Key Laboratory of Agricultural Products Processing, Sericultural & Agri-food Research Institute, Guangdong Academy of Agricultural Sciences, Guangzhou 510610, China;2. College of Food Science and Biology, Hebei University of Science and Technology, Shijiazhuang 050018, China; 3. Guangdong Tianzhiyuan Agriculture Science and Technology Co. Ltd., Jiangmen 529100, China)
  • Online:2022-05-25 Published:2022-05-27

摘要: 以“仲甜9号”、“珠玉甜8号”、“珠玉甜1号”3 个品种甜玉米为材料,研究甜玉米籽粒成熟过程中挥发性风味物质的变化规律。采用顶空固相微萃取-气相色谱-质谱联用分析技术,结合NIST14质谱数据库比对、保留指数分析、气相色谱嗅闻分析等方法对挥发性风味物质进行鉴定,利用内标法测定其含量,构建甜玉米挥发性风味活性化合物组成谱,评价甜玉米香气品质与特征。结果表明:3 种甜玉米在成熟过程中共检测到61 种挥发性风味物质;成熟度对挥发性风味物质种类和含量有显著影响,随成熟度增加,壬酸乙酯、1-庚醇、1-己醇含量显著下降,苯乙烯、甲苯、乙苯、1,3-二甲基苯含量显著增加,籽粒成熟过程中以积累芳香烃为主。在气味特征方面,随着籽粒的成熟,脂香强度明显增强,青香强度明显减弱。甜玉米品种之间存在差异,“仲甜9号”甜玉米成熟期时挥发性风味物质种类和含量明显高于其他2 个品种,且整体风味强度最大。

关键词: 甜玉米;成熟;挥发性风味物质;气味强度;变化规律

Abstract: The changes of volatile flavor compounds in three varieties of sweet corn, “Zhongtian 9”, “Zhuyutian 8” and “Zhuyutian 1”, were investigated during the ripening process. The volatile flavor compounds were identified by headspace solid phase microextraction and gas chromatography-mass spectrometry (HS-SPME-GC-MS) through NIST14 mass spectral database searching and retention index analysis as well as by gas chromatography-olfactory (GC-O), and were quantified by the internal standard method, in order to construct a volatile flavor profile and evaluate the aroma characteristics of sweet corn. The results showed that 61 volatile flavor compounds were detected across the three varieties during the ripening process. Maturity had significant effects on the type and content of volatile flavor compounds in sweet corn. The contents of ethyl nonylate, 1-heptanol and 1-hexanol significantly decreased with increasing maturity, while the contents of styrene, toluene, ethylbenzene and m-xylene significantly increased. Arenes were mainly accumulated in sweet corn during the maturation process. In terms of odor characteristics, the intensity of fatty aroma increased obviously with maturity, while the intensity of grassy aroma decreased obviously. There were significant differences among varieties in the composition and content of volatile flavor compounds. The number and amount of volatile flavor compounds in “Zhongtian 9” were significantly greater than those in the other two varieties at maturity, and the overall flavor intensity was the highest.

Key words: sweet corn; ripening; volatile flavor compounds; odor intensity; changing pattern

中图分类号: