食品科学 ›› 2023, Vol. 44 ›› Issue (24): 339-345.doi: 10.7506/spkx1002-6630-20221201-008

• 安全检测 • 上一篇    下一篇

基于两种检测方法对特膳食品渗透压测定的比对

潘丽蓉, 吴媛, 赵子彦, 袁文萱, 方恩华, 徐敦明   

  1. (厦门海关技术中心,福建 厦门 361013)
  • 出版日期:2023-12-25 发布日期:2024-01-02
  • 基金资助:
    “十三五”国家重点研发计划重点专项(2019YFC1605400)

Comparison of Two Methods for Osmolality Determination of Foods for Special Dietary Uses

PAN Lirong, WU Yuan, ZHAO Ziyan, YUAN Wenxuan, FANG Enhua, XU Dunming   

  1. (Xiamen Customs Technical Center, Xiamen 361013, China)
  • Online:2023-12-25 Published:2024-01-02

摘要: 对收集的市售9 种类型特殊膳食用食品,共46 个样品,分别采用渗透压冰点检测仪器和渗透压露点检测仪器进行测定,比对分析方法间的差异性。结果表明,市售特殊膳食用食品在冰点仪器检测范围为195~763 mOsmol/kg,相对标准偏差(relative standard deviation,RSD)为0.20%~4.08%;露点法检测范围为197~649 mmol/kg,RSD为0.00%~3.66%。本研究发现不同冲泡方式对测定结果具有显著影响,溶液温度也会影响测定结果的平行性。针对同一样品的两种测定方法结果进行统计学分析(采用t检验法),结果表明:31 个样品的两种测定方法差异显著。通过实验研究推断,样品溶液是否达到理想稀溶液状态是影响两种方法存在显著差异的主要因素。本研究为特殊膳食用食品中渗透压检测情况的后续研究提供理论基础和方向,还可以为特殊膳食用食品的产品生产设计过程提供一些亟需注意的关键点,为国民健康食品的开发提供一定的理论基础。

关键词: 冰点法;露点法;t检验;特殊膳食用食品?

Abstract: A total of 46 samples from nine types of commercially available foods for special dietary uses were collected for osmolality measurement by a freezing point and a dew point osmometer, and the differences between the two methods were analysed. The results showed that the detection range of the freezing point osmometer was 195–763 mOsmol/kg with relative standard deviation (RSD) of 0.20%–4.08%, and the detection range of the dew point osmometer was 197–649 mmol/kg with RSD of 0.00%–3.66%. It was found that different reconstitution methods had a significant effect on the determination results, and the temperature of the solution also affected the parallelism of the determination results. Statistical analysis using t-test showed that there were significant differences between the results of the two methods for each of 31 samples. It was inferred from the experiments that whether the sample solution reached an ideal dilute solution state was the major factor affecting the significant difference between both methods. This study provides a theoretical basis for further research on the detection of osmolality in foods for special dietary uses, and highlights some key issues that need urgent attention in the design and production of foods for special dietary uses.

Key words: freezing point osmometer; dew point osmometer; t-test; food for special dietary use

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