Determination of Quinolone Residues in Royal Jelly by High-Performance Liquid Chromatography Coupled with luorescence Detector

doi:10.7506/spkx1002-6630-200906051

FOOD SCIENCE ›› 2009, Vol. 30 ›› Issue (6): 222-225.doi: 10.7506/spkx1002-6630-200906051

Previous Articles Next Articles

Determination of Quinolone Residues in Royal Jelly by High-Performance Liquid Chromatography Coupled with luorescence Detector

ZHOU Ping1，HU Fu-liang2,*，XU Quan-hua1，SHAO Qiao-yun1

(1. Zhejiang Beewords Apiculture Group Co. Ltd., Tonglu 311500, China；
2. College of Animal Science, Zhejiang University, Hangzhou 310029, China)

Received:2008-05-05 Revised:2008-07-04 Online:2009-03-15 Published:2010-12-29
Contact: HU Fu-liang2,* E-mail:flhu@zju.edu.cn; fulianghu@yahoo.com

Abstract

Abstract:

Quinolones (QNs) is one kind of antibiotics, and in recent years its residue exceeding limits has been found frequently n animal-origin exportation food such as bee products. In this study, liquid-liquid extraction was used to pre-treat royal jelly ample, and then five QNs residues in royal jelly sample were determined by high-performance liquid chromatography coupled ith fluorescence detector. The results showed that the detection limits of ofloxacin, enrofloxacin, ciprofloxacin, norfloxacin and anofloxacin are 5 μg/kg, 2.5 μg/kg, 2.5 μg/kg, 2.5 μg/kg and 1 μg/kg, respectively, which meet the detection demand of allowable imits of QNs in royal jelly. The proposed method is simple, rapid, accurate and low-reagent consumption and cost.

Key words: high-performance liquid chromatography coupled with fluorescence detector, oyal jelly, quinolones, residue

CLC Number:

S859.84

ZHOU Ping1，HU Fu-liang2,*，XU Quan-hua1，SHAO Qiao-yun1. Determination of Quinolone Residues in Royal Jelly by High-Performance Liquid Chromatography Coupled with luorescence Detector[J]. FOOD SCIENCE, 2009, 30(6): 222-225.

[1]	ZHU Xiaoling, LIU Jie, YU Tingting, ZHANG Li, WANG Huixia, WU Wanqin, CAO Qi, ZHANG Yazhen, YANG Zong. Rapid Screening of Pesticide Residues in Pepper Powder by High Performance Liquid Chromatography Coupled with Quadrupole-Time of Flight Mass Spectrometry [J]. FOOD SCIENCE, 2021, 42(4): 287-296.
[2]	LIAN Yujing, ZHOU Yiran, SUN Xin, CHEN Jianan, ZHENG Zhenjia, WANG Minglin. Development of a Modified QuEChERS Method Based on Amine-Functionalized Iron Oxide Nanoparticles for the Simultaneous Determination of Seven Pesticides in Fruits and Vegetables by GC-MS/MS [J]. FOOD SCIENCE, 2021, 42(4): 297-304.
[3]	FU Ruijie, ZHOU Jing, TIAN Fengyu, JIAO Bining, HE Yue. Recent Progress in Nanomaterial-Based Optical Aptasensors for the Detection of Pesticide Residues [J]. FOOD SCIENCE, 2021, 42(3): 330-338.
[4]	ZHAO Lei, PAN Fei, LIN Wenxuan, XU Meili, BAO Xi, CHEN Yanlin, WANG Chengtao, LIAN Yunhe. Main Components of Stevia Residue Extract and Their Antioxidant Activities [J]. FOOD SCIENCE, 2021, 42(2): 247-254.
[5]	LIU Fengyin, LI Ying, WANG Xiaopeng, WU Xiaodan, CHEN Fengyan, LIANG Yue, YUAN Xuewen, MU Hongtao. An Enzyme Inhibition Method for Rapid Multi-residue Determination of β-Lactamase Inhibitors in Milk [J]. FOOD SCIENCE, 2021, 42(14): 248-254.
[6]	ZHONG Haowen, YANG Guoshun, CHEN Wenting, BAI Miao, TAN Jun. Determination and Pollution Characteristics of 33 Pesticide Residues in Grapes by GC-QqQ-MS/MS with Stable Isotope Internal Standard [J]. FOOD SCIENCE, 2021, 42(14): 263-269.
[7]	SHU Xiao, CHU Nengming, ZHANG Xuemei, MENG Xia, LI Dianyan, HUANG Chenglan, XIANG Jia, YANG Junying. Rapid Determination of 62 Pesticide Residues in Chicken Eggs by Enhanced Matrix Removal of Lipids Combined with Gas Chromatography-Tandem Mass Spectrometry [J]. FOOD SCIENCE, 2021, 42(14): 320-327.
[8]	BAI Xue, CHEN Yu, ZHAO Lijun, ZHANG Jing. Residual Pattern and Predicting Modeling of Florfenicol in Eggs and Body Tissues of Laying Hens [J]. FOOD SCIENCE, 2021, 42(13): 26-33.
[9]	ZOU Ying, YU Yuanshan, ZOU Bo, CHENG Lina, XIAO Gengsheng, WU Jijun, BU Zhibin, XU Yujuan. Preparation and Stability of Freeze-Dried Polyphenol Extracted from Mulberry Juice Processing Residues [J]. FOOD SCIENCE, 2021, 42(1): 73-78.
[10]	LIANG Xiumei, ZHANG Weiyi, ZHANG Wei, XIE Shibing, HE Ruyi, XU Jing, SU Laijin, SUN Bolun, ZHANG Jing. Simultaneous Determination of Residues of 38 Pesticides in Fruits by QuEChERS Combined with High Performance Liquid Chromatography-Tandem Mass Spectrometry [J]. FOOD SCIENCE, 2020, 41(8): 288-296.
[11]	TONG Litao, JU Zhiyuan, GENG Donghui, WANG Lili, ZHOU Xianrong, ZHOU Sumei. Rice Vinegar Residue Reduces Adipocyte Size and Hyperlipidemia by Inhibiting Lipids Absorption in Hamsters [J]. FOOD SCIENCE, 2020, 41(5): 128-134.
[12]	MENG Yong, WANG Jing, ZHU Xiaohua, GENG Xuebing, YANG Zong, SHEN Meifang. Screening and Confirmation of Multiple Antibiotic Residues in Aquatic Products by Triple Quadrupole-Linear Ion Trap Mass Spectrometry [J]. FOOD SCIENCE, 2020, 41(4): 313-318.
[13]	ZHANG Qinjun, BEI Ronghua, ZHANG Hong, HU Changying. Determination of Residues and Migration of 17 Acrylate Monomers in Food Composite Packaging Materials by Gas Chromatography-Mass Spectrometry [J]. FOOD SCIENCE, 2020, 41(24): 287-294.
[14]	LIU Weihua, YANG Xi, LIU Minxuan, YU Wenlong, WANG Xianghong. Development of an Electrochemical Immunosensor for Rapid Quantification of Florfenicol in Animal-Derived Foods [J]. FOOD SCIENCE, 2020, 41(20): 307-313.
[15]	TONG Jixu, ZHU Zhiqiang, QIAN Yongzhong. SO2 Residue and Potential Dietary Health Risk Assessment in Grapes under Different Storage Conditions [J]. FOOD SCIENCE, 2020, 41(1): 163-167.

Determination of Quinolone Residues in Royal Jelly by High-Performance Liquid Chromatography Coupled with luorescence Detector

RichHTML

PDF (PC)

Knowledge

Abstract

Cite this article

share this article

References

Related Articles 15

Recommended Articles

Metrics

Comments