Proximate Nutritional Composition and Volatile Aroma Compounds of Rosa sterilis S. D. Shi Fruits from Different Growing Areas of Guizhou Province

doi:10.7506/spkx1002-6630-201622025

Abstract

Abstract: Objective: This study aimed to investigate the difference in proximate nutritional composition and volatile aroma compounds of Rosa sterilis S. D. Shi fruits from different growing areas of Guizhou province. Methods: Characters and contents of basic ingredients of Rosa sterilis S. D. Shi collected from four regions of Guizhou were first evaluated. The organic acid compositions were then analyzed by high performance liquid chromatography (HPLC) and volatile compounds were determined by gas chromatography-mass spectrometry (GC-MS). Results: Rosa sterilis S. D. Shi from Anshun and Xingyi were much higher in weight and diameter than others. Fruits from Xingyi were much higher in L* than others. Rosa sterilis S. D. Shi from Anshun exhibited the highest level of superoxide dismutase (SOD) and VC contents; Fruits from Guiyang had the highest content of polyphenols and those from Anshun and Guiyang were much higher in the water content than others. There were no significant differences in other ingredients. Six organic acids were found in Rosa sterilis S. D. Shi, with citric acid and ascorbic acid being the most abundant. Rosa sterilis S. D. Shi from four growing areas contained a total of 60 aroma compounds, i.e. Anshun, 42; Guiyang, 39; Shibing, 49; and Xingyi, 40, among which, D-limonene, α-guaiene, isoamyl acetate, ethyl caprylate, ethyl n-hexoate, leaf acetate, benzaldehyde and 2,6,10,10-tetramethyl-1-oxa-spiro[4.5]dec-6-ene were the most important ones. Conclusions: Rosa sterilis S. D. Shi from four growing areas have significant differences in characters, basic ingredients and aroma compounds.

Key words: Rosa sterilis S. D. Shi, fruit character, basic ingredients, organic acid, volatile aroma compounds

CLC Number:

TS255.2

ZHANG Dan, WEI Guangxin, ZENG Fankun,*. Proximate Nutritional Composition and Volatile Aroma Compounds of Rosa sterilis S. D. Shi Fruits from Different Growing Areas of Guizhou Province[J]. FOOD SCIENCE, 2016, 37(22): 166-172.

References

[1] JANSE R C, ERASMUS E, LOOTS D T, et al. Rosa roxburghii supplementation in a controlled feeding study increases plasma antioxidant capacity and glutathione redox state[J]. European Journal of Nutrition, 2005, 44: 452-457. DOI:10.1007/s00394-005-0555-x.
[2] 吴洪娥, 金平, 周艳, 等. 刺梨与无籽刺梨的果实特性及其主要营养成分差异[J]. 贵州农业科学, 2014, 42(8): 221-223. DOI:10.3969/j.issn.1001-3601.2014.08.059.
[3] 鲁敏, 安华明, 赵小红. 无籽刺梨与刺梨果实中氨基酸分析[J]. 食品科学, 2015, 36(14): 118-121. DOI:10.7506/spkx1002-6630-2015140023.
[4] 陈发兴, 刘星辉, 陈立松. 果实有机酸代谢研究进展[J]. 果树学报, 2005, 22(5): 526-531. DOI:10.3969/j.issn.1009-9980.2005.05.020.
[5] 罗安才, 杨晓红, 邓英毅, 等. 柑橘果实发育过程中有机酸含量及相关代谢酶活性的变化[J]. 中国农业科学, 2003, 36(8): 941-944. DOI:10.3321/j.issn:0578-1752.2003.08.014.
[6] 牛景, 赵剑波, 吴本宏, 等. 不同来源桃种质果实糖酸组分含量特点的研究[J]. 园艺学报, 2006, 33(1): 6-11. DOI:10.3321/j.issn:0513-353X.2006.01.002.
[7] 成冰, 张京芳, 徐洪宇, 等. 不同品种酿酒葡萄有机酸含量分析[J]. 食品科学, 2013, 34(12): 223-228. DOI:10.7506/spkx1002-6630-201312046.
[8] 安华明, 刘明, 杨曼, 等. 刺梨有机酸组分及抗坏血酸含量分析[J]. 中国农业科学, 2011, 44(10): 2094-2100. DOI:10.3846/j.issn.0578-175.2011.10.014.
[9] 姜永新, 高健, 赵平, 等. 无子刺梨新鲜果实挥发性成分的GC-MS分析[J]. 食品研究与开发, 2013, 34(14): 91-94.
[10] 付慧晓, 王道平, 黄丽荣, 等. 刺梨和无籽刺梨挥发性香气成分分析[J]. 精细化工, 2012, 29(9): 875-878. DOI:10.13550/j.jxhg.2012.09.020.
[11] 李里特. 食品物性学[M]. 北京: 中国农业出版社, 1998. [12] 姜微波, 曹健康, 赵玉梅. 果蔬采后生理生化实验指导[M]. 北京: 中国轻工业出版社, 2007.
[13] 刘畅, 王秋红, 方波, 等. 刺梨黄酮提取工艺研究[J]. 食品工业, 2010, 31(1): 52-54.
[14] 夏宏义, 杨勇, 夏乐晗, 等. 柿果成熟过程中总酚和缩合单宁含量的变化[J]. 食品科学, 2014, 35(19): 16-71. DOI:10.7506/spkx1002-6630-201419014.
[15] 刘二先. 木瓜超氧化物歧化酶, 黄酮及齐墩果酸的综合提取初探[D]. 武汉: 华中科技大学, 2007.
[16] 成冰, 张京芳, 徐洪宇, 等. 不同品种酿酒葡萄有机酸含量分析[J]. 食品科学, 2013, 34(12): 223-228. DOI:10.7506/spkx1002-6630-201312046.
[17] FAN W, QIAN M C. Characterization of aroma compounds of Chinese “Wuliangye” and “Jiannanchun” liquors by aroma extract dilution analysis[J]. Journal of Agricultural and Food Chemistry, 2006, 54(7): 2695-2704. DOI:10.1021/jf052635t.
[18] 史肖白, 庄一义. 刺梨超氧化物歧化酶含量分析[J]. 中国野生植物资源, 1998, 17(4): 49-50.
[19] 赵金梅, 高贵田, 薛敏, 等. 不同品种猕猴桃果实的品质及抗氧化活性[J]. 食品科学, 2014, 35(9): 118-122. DOI:10.7506/spkx1002-6630-201409024.
[20] 刘世尧. 不同产区皱皮木瓜有机酸组成及主要活性成分分离纯化研究[D]. 重庆: 西南大学, 2012.
[21] 范文来. 酒类风味化学[M]. 北京: 中国轻工业出版社, 2014.
[22] 乔宇, 谢笔钧, 张妍, 等. 三种温州蜜柑果实香气成分的研究[J]. 中国农业科学, 2008, 41(5): 1452-1458.
[23] CABRITA M J, FREITAS A M C, LAUREANO O, et al. Glycosidic aroma compounds of some Portuguese grape cultivars[J]. Journal of the Science of Food and Agriculture, 2006, 86(6): 922-931. DOI:10.1002/jsfa.2439.
[24] PLOTTO A, MARGARIA C A, GOODNER K L, et al. Odour and ?avour thresholds for key aroma components in an orange juice matrix: terpenes and aldehydes[J]. Flavour and Fragrance Journal, 2004, 19(6): 491-498. DOI:10.1002/ffj.1470.
[25] 李小林, 陈诚, 清源, 等. 会东县不同品种块菌挥发性香气成分的 GC-MS 分析[J]. 食品科学, 2015, 36(18): 132-136. DOI:10.7506/spkx1002-6630-201518024.
[26] 高婷婷, 韩帅, 刘玉平, 等. 固相微萃取结合GC-MS分析鲜山楂果肉中的挥发性成分[J]. 食品科学, 2013, 34(20): 144-147. DOI:10.7506/spkx1002-6630-201320029.
[27] DIXON J, HEWETT E W. Factors affecting apple aroma/flavour volatile concentration: a review[J]. New Zealand Journal of Crop and Horticultural Science, 2000, 28(3): 155-173. DOI:10.1080/01140671.2000.9514136.
[28] 刘长辉, 雷存喜, 顾浩, 等. 茶螺烷的合成[J]. 化学试剂, 2010, 32(4): 362-364. DOI:10.3969/j.issn.0258-3283.2010.04.023.