FOOD SCIENCE ›› 2007, Vol. 28 ›› Issue (6): 274-277.

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Study on Rapid Determination of Trace-copper in Nanyang Color Wheat Flour

 GAO  Xiang-Yang, RAN  Hui-Hui, WANG  Kun, GONG  An-Jing   

  1. 1.College of Food Science and Technology, Henan Agricultural University, Zhengzhou 450002, China; 2.Quality Supervision Office of Baoding City, Baoding 071000, China
  • Online:2007-06-15 Published:2011-12-31

Abstract: Objective: To establish a new determination method of trace-copper in Nanyang color wheat. Methods: Selecting Nanyang grey wheat, blue wheat, common violet wheat, viotet hard-wheat and Zhou wheat 16 as the raw materials, copper-selective electrode with direct reading concentration method was adopted. It compared it with the China Standard (GB/T5009.13-2003) for determining trace copper in Nanyang color wheat, after the samples being digested by high- pressure microwave. Results: The recovery is in range 86.5%~102.0% by standard addition method. The relative stan- dard deviations(RSD) is between 1.1%~3.1%(n=11). The lowest detection limit of copper is 0.0026 mg/L. The linear range is 0.032~65 mg/L. Conclusions: This method is found to be direct-reading, quick, simple, sensitive and accurate. The analytical results are satisfactory.

Key words: ion-selective electrode, direct-reading concentration method, trace-copper, microwave digestion, Nanyang color wheat flour, rapid determination