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Uncertainty Evaluation for the Determination of Bifenthrin in Tea by Gas Chromatography and Gas Chromatography-Mass Spectrometry

WANG Ji-xiang, ZHANG Xue-zhong, WANG Ya-qin, NIU Zhi-rui, FENG Lei, ZHAO Yu   

  1. Yunnan Product Quality Supervision and Testing Academy, Kunming 650223, China
  • Online:2014-06-25 Published:2014-07-03

Abstract:

The possible uncertainties in the determination of bifenthrin in tea by gas chromatography (GC) and gas
chromatography-mass spectrometry (GC-MS) were analyzed and evaluated. According to Evaluation and Expression
of Uncertainty in Measurement (JJF 1059—1999), a mathematical model of uncertainty was established. Based on the
contribution ratio of each uncertainty component to the synthetic uncertainty, the key uncertainties resulted from sample
pretreatment and calibration curve preparation.

Key words: gas chromatography (GC), gas chromatography-mass spectrometry (GC-MS), bifenthrin, uncertainty, tea

CLC Number: