食品科学

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热辐气动干燥法快速测定牛奶中总固体和水分

赵 敏,周 聪*   

  1. 中国热带农业科学院分析测试中心,海南省热带果蔬产品质量安全重点实验室,海南 海口 571101
  • 出版日期:2015-01-25 发布日期:2015-01-16
  • 通讯作者: 周 聪
  • 基金资助:

    海南省自然科学基金项目(314096)

Rapid Determination of Total Solids and Water in Milk by Hot Radiation Pneumatic Drying Method

ZHAO Min, ZHOU Cong*   

  1. Hainan Provincial Key Laboratory of Quality and Safety for Tropical Fruits and Vegetables, Analysis and Testing Center,
    Chinese Academy of Tropical Agricultural Sciences, Haikou 571101, China
  • Online:2015-01-25 Published:2015-01-16
  • Contact: ZHOU Cong

摘要:

利用圆盘自动进样热辐箱式胶乳样品干燥仪研究快速测定牛奶中总固体和水分含量的方法。分别对加热温度、加热时间及温度平衡时间进行实验,以烘箱法(标准法)为对照,不断优化实验条件,并测定了多份牛奶样品中总固体和水分的含量。结果表明:用本方法和烘箱法测定相同样品中总固体和水分含量的准确度和精确度结果一致,而烘箱法需耗时约3.5 h,本方法只需2.0 min完成,大大提高了分析效率。

关键词: 热辐气动干燥, 牛奶, 总固体, 水分

Abstract:

A latex sample drying apparatus with a hot radiation box for automatically injecting samples by discs is applied
for the rapid determination of total solids and water content in milk. Important experimental conditions, such as temperature,
heating time and temperature equilibration method, were optimized using an oven drying method (a standard method) as
control for the determination of total solids and water contents in various milk samples. The results showed that the same
accuracy and precision were achieved for the determination of total solids and water contents in one sample by the proposed
method and oven drying method. The drying time required for oven drying method was 3.5 hours, compared to only
2.0 minutes for our method as a more efficient method. Therefore, a novel, simple, rapid, stable and reliable method to
determine total solids and water contents in fresh milk has been established.

Key words: hot radiation pneumatic drying apparatus, milk, total solids, water contents

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