食品科学 ›› 2017, Vol. 38 ›› Issue (11): 103-109.doi: 10.7506/spkx1002-6630-201711017

• 基础研究 • 上一篇    下一篇

低场核磁共振技术研究猪肉冷却过程中水分迁移规律

张 楠,庄昕波,黄子信,陈玉仑,李春保,周光宏   

  1. 南京农业大学 肉品加工与质量控制教育部重点实验室,农业部畜产品加工重点实验室,江苏省肉类生产与加工质量安全控制协同创新中心,江苏 南京 210095
  • 出版日期:2017-06-15 发布日期:2017-06-19

Change in Water Mobility in Pork during Postmortem Chilling Analyzed by Low-Field Nuclear Magnetic Resonance

ZHANG Nan, ZHUANG Xinbo, HUANG Zixin, CHEN Yulun, LI Chunbao, ZHOU Guanghong   

  1. Key Laboratory of Meat Products Processing and Quality Control, Ministry of Education, Key Laboratory of Animal Products Processing, Ministry of Agriculture, Jiangsu Synergetic Innovation Center of Meat Processing and Quality Control, Nanjing Agricultural University, Nanjing 210095, China
  • Online:2017-06-15 Published:2017-06-19

摘要: 目的:采用低场核磁弛豫时间和低场核磁成像技术,研究在模拟冷库环境条件下,风循环冷却和雾化喷淋冷却过程中猪肉水分迁移规律。方法:选择宰后2 h内的整条带皮猪背最长肌(通脊)10 条,沿肌肉走向垂直方向分切成4 份14 cm×10 cm×6 cm的肉块,其中2 份保留猪皮及皮下脂肪(带皮组),另2 份则去除猪皮及皮下脂肪(不带皮组),带皮组和不带皮组肉块分别放入风循环冷却和雾化喷淋冷却的模拟冷库中进行冷却,并于0.0、1.5、3.0、4.5、6.0 h和7.5 h进行低场核磁共振横向弛豫时间(T2)和低场核磁成像测定,同时记录肉块质量变化。结果:风循环冷却过程中猪肉中结合水峰面积A2b和结合水占猪肉中总水分的百分比P2b变化差异不显著(P>0.05)、不易流动水t21显著降低(P<0.05),自由水A22、P22也显著降低(P<0.05);而在雾化喷淋冷却过程中,结合水A2b、P2b和不易流动水t21、A21、P21变化差异不显著(P>0.05),自由水A22、P22则显著降低(P<0.05)。带皮猪肉和不带皮猪肉在冷却过程中水分迁移的变化过程相同,但水分损耗存在差异。结合图像分析,在冷却过程初期,猪肉干耗主要是自由水的损失;而冷却后期,猪肉干耗则主要是部分不易流动水的损失。雾化喷淋冷却通过补充外源水,来减小猪肉内部和外表的水势差而抑制不易流动水由内向外迁移,可有效降低冷却干耗。

关键词: 低场核磁弛豫时间, 低场核磁成像, 冷却干耗, 雾化喷淋冷却, 风循环冷却

Abstract: Objective: This study was designed to explore the change in water mobility in skin-on and skin-off pork during blast chilling and spray chilling. Methods: Ten skin-on pork loins were obtained at 2 h postmortem and each loin was cut into 4 steaks (14 cm × 10 cm × 6 cm), the skin of two of which was kept and the other two were skinless. Skin-on and skinless steaks were individually subjected to blast chilling and spray chilling. At 0.0, 1.5, 3.0, 4.5, 6.0 and 7.5 h of chilling, transverse relaxation time (T2) and magnetic resonance images (MRI) were determined by low-field nuclear magnetic resonance (LF-NMR) and sample weight was measured. Results: The A2b and P2b changed without statistical significance (P > 0.05), and the t21, A22 and P22 were significantly decreased during blast chilling (P < 0.05), while spray treatment significantly reduced A22 and P22 (P < 0.05), but it had no significant effect on A2b, P2b, t21, A21 or P21 (P > 0.05). The water mobility in skinless or skin-on pork under two chilling treatments was similar, while the evaporative loss was significantly affected by the treatments (P < 0.05). At the initial stage of blast chilling, the evaporative loss was mainly derived from free water, while it was immobilized water that contributed to the evaporative loss at the late stage. The spray chilling treatment could replace the immobilized water during the removal of heat from pork, resulting in a reduction of evaporative loss.

Key words: low-field nuclear magnetic relaxation time, low-field nuclear magnetic resonance imaging, evaporative loss, spray chilling, blast chilling

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