Analysis of Volatile Compounds in Foie Gras by SDE, GC-MS and GC-O

Abstract

Abstract: The volatile compounds in foie gras was extracted by simultaneous distillation extraction (SDE) and analyzed by gas chromatography-mass spectrometry (GC-MS) and gas chromatography-olfactometry (GC-O). Totally 41 volatile flavor compounds were identified including 8 hydrocarbons, 4 alcohols, 2 phenols 7 aldehydes, 5 ketones, 1 acids, 7 ester, 7 other compounds and 3 unknown compounds. Among these compounds, hexanal, 2-ethylcyclohexanol, nonanal, 2-pentadecanone, 6,10,14-trimethyl-tetradecanal, di-n-octyl phthalate made a greater contribution to the flavor of foie gras.

Key words: foie gras, simultaneous distillation extraction (SED), gas chromatography-mass spectrometry (GC-MS), gas chromatography-olfactometry (GC-O), volatile flavor constituents

CLC Number:

TS251.2

Xie ZhangBin. Analysis of Volatile Compounds in Foie Gras by SDE, GC-MS and GC-O[J]. FOOD SCIENCE, 0, (): 220-223.

References

[1]周敏.null潘健存, 王土长. 鹅肝酱的营养作用及其生产技术[J].广西农学报,2004,:-
[2]高原.鹅肥肝与心脏病[J ][J].中国家禽,2001,23(7):27-
[3]郭建辉, 刘安军, 刘有志, 等.高效液相法测定鹅肥肝和鹅肝酱中维生素A[J].食品研究与开发,2006,27(10):113-115
[4]赵文红.null刘锐, 白卫东, 等. 鹅肝酱的研制[J].. 农产品加工: 学刊,2007,:-
[5]綦艳梅, 孙宝国, 黄明泉, 等.同时蒸馏萃取-气质联用分析月盛斋酱牛肉的挥发性风味成分[J].食品科学,2010,31(18):471-372
[6]赵庆喜, 薛长湖, 徐杰, 等.微波蒸馏-固相微萃取-气相色谱-质谱-嗅觉检测器联用分析鳙鱼鱼肉中的挥发性成分[J].色谱,2010,25(2):267-271
[7]侯园园, 王兴国, 刘元法.GC-O与GC- MS结合鉴定天然乳脂风味中的特征致香成分[J].食品工业科技,2008,29(3):143-145
[8]Sophie Le Guen, Carole Prost , Michel Demaimay.Evaluation of the representativeness of the odor of cooked mussel extracts and relationsh ip between sensory description and potent odorants[ J][J].J Agric Food Chem,2001,49:1321-1327
[9]李桂花.null何巧红, 杨君. 一种提取复杂物质中易挥发组分的有效方法-同时蒸馏萃取及其应用[J].. 理化检验: 化学分册,2009,:-
[10]XIE Jianchun, SUN Baoguo, WANG Shuaibin.Aromatic constituents from Chinese traditional smoke-cured bacon of Mini-pig[J].Food Science and Technology International,2008,14(4):329-340
[11]Lin J, Rouseff R L.Characterization of aroma-impact compounds in cold-pressed grapefruit oil using time-intensity GC-O and GC-MS[J].Flavour Fragrance J,2001,16:457-463
[12]Jezussek M.Comparison of key aroma compounds in cooled brown rice varieties based on aroma extract dilution analysis[ J][J].J Agric Food Chem,2002,50(5):1101-1105
[13]Qian M, Reineccius G.Potent aroma compounds in Parmigiano Reggiano cheese studied using a dynamic head space(purge-trap) method[ J][J].Flavour FragranceJ,2003,18(3):252-259
[14]马永昆, 李祥波, 蒋家奎.基于GC-MS和嗅闻仪联用的天然苹果香精关键香气成分分析[J].食品科学,2009,30(8):231-234

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