食品科学

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响应面分析法优化超声波提取干制红枣中大位阻农药三唑锡工艺

田木星,王伟华*,涂 玲   

  1. 塔里木大学生命科学学院,新疆生产建设兵团南疆特色农产品深加工重点实验室,新疆 阿拉尔 843300
  • 出版日期:2015-02-25 发布日期:2015-02-16
  • 通讯作者: 王伟华
  • 基金资助:

    新疆生产建设兵团博士资金项目(2012BB012);国家级大学生创新创业训练计划项目(2013107570010)

Optimization of Ultrasonic-assisted Solvent Extraction Process for Azocyclotin from Dried Jujube by Response Surface Analysis

TIAN Muxing, WANG Weihua*, TU Ling   

  1. Xinjiang Production and Construction Corps Key Laboratory of Deep Processing of Agricultural Products in South Xinjiang,
    College of Life Science, Tarim University, Alar 843300, China
  • Online:2015-02-25 Published:2015-02-16
  • Contact: WANG Weihua

摘要:

以干制红枣为材料,研究超声波辅助法提取大位阻农药三唑锡的最佳条件。考察超声提取功率、提取温度、提取时间、料液比及提取次数5 个单因素对三唑锡提取的影响,并在单因素试验的基础上进行响应面分析,得到三唑锡提取的最佳工艺条件为温度45 ℃、频率45 kHz、料液比1∶12(g/mL)、提取6 次、提取时间50 min、超声提取功率70 W,经验证,此条件下三唑锡含量为0.15 mg/kg。

关键词: 超声提取, 红枣, 三唑锡

Abstract:

The present work was undertaken to investigate optimal conditions for ultrasonic-assisted extraction azocyclotin
from dried jujube. The effects of five factors including ultrasonic power, extraction temperature, extraction time, solid-toliquid
ratio and extraction number on extraction efficiency were explored using a combination of single factor method and
response surface methodology. An extraction temperature of 45 ℃, an ultrasonic frequency of 45 kHz, an ultrasonic power
of 70 W and 50 min extractions performed six times with a solid-to-liquid ratio of 1:12 (g/mL) were selected as the optimal
extraction conditions. Experiments conducted under these conditions resulted in an extraction rate of 0.15 mg/kg.

Key words: ultrasonic-assisted extraction, jujube, azocyclotin

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