食品科学 ›› 2020, Vol. 41 ›› Issue (18): 203-209.doi: 10.7506/spkx1002-6630-20200119-232

• 成分分析 • 上一篇    下一篇

卤汤牛肉贮藏过程中挥发性风味物质分析

李素,周慧敏,赵冰,潘晓倩,朱宁,吴倩蓉,刘梦,张顺亮   

  1. (中国肉类食品综合研究中心,肉类加工技术北京市重点实验室,北京 100068)
  • 出版日期:2020-09-25 发布日期:2020-09-18
  • 基金资助:
    “十三五”国家重点研发计划重点专项(2017YFD0400105-03)

Analysis of Volatile Flavor Compounds in Stewed Beef with Broth during Storage

LI Su, ZHOU Huimin, ZHAO Bing, PAN Xiaoqian, ZHU Ning, WU Qianrong, LIU Meng, ZHANG Shunliang   

  1. (Beijing Key Laboratory of Meat Processing Technology, China Meat Research Center, Beijing 100068, China)
  • Online:2020-09-25 Published:2020-09-18

摘要: 以卤汤牛肉为研究对象,采用吹扫捕集-热脱附-气相色谱-质谱联用法,结合气味活度值(odor activity value,OAV)及主成分分析(principal component analysis,PCA)法分别分析牛肉及肉汤在贮藏期间(0、2、4、6、8 月)挥发性风味物质变化情况。结果表明:牛肉及肉汤挥发性风味物质变化规律不同,牛肉样品中挥发性风味物质总含量在贮藏4?个月时最高(5?380.24?μg/kg),肉汤样品中2?个月时含量最高(3?877.84?μg/kg);样品中醇类物质含量最高,其次是醛类物质,其中壬醛差异最大。OAV分析可知,醛类物质是主要风味贡献物质,结合PCA发现壬醛、辛醛、对茴香醛是卤汤牛肉样品的主要风味贡献物质。

关键词: 卤汤牛肉;主成分分析;气味活度值;贮藏;挥发性风味物质

Abstract: Changes in the volatile flavor compounds of stewed beef with broth stored for different periods (0, 2, 4, 6, and 8 months) were analyzed using purge and trap-thermal desorption-gas chromatography-mass spectrometry combined with odor activity and principal component analysis (PCA). The results showed that the patterns of change in volatile flavor compounds were different between the beef and the broth. The total content of volatile flavor compounds in the beef was the highest up to 5 380.24 μg/kg when stored for 4 months. The maximum total content (3 877.84 μg/kg) of volatile flavor compounds in the broth sample was reached after 2 months of storage. Alcohols were the most abundant volatile compounds for both samples, followed by aldehydes, and the content of nonanal showed the biggest difference between the two samples. Odor activity value (OAV) analysis showed that aldehydes were the main flavor contributors. PCA analysis indicated that nonanal, octanal and p-anisaldehyde were the main flavor contributors of stewed beef samples.

Key words: stewed beef with broth; principal component analysis; odor activity value; storage; volatile flavor compounds

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