食品科学 ›› 2020, Vol. 41 ›› Issue (16): 202-209.doi: 10.7506/spkx1002-6630-20200121-258

• 成分分析 • 上一篇    

模糊数学评价优化浓香花生油脂体的预处理参数及香气成分分析

魏松丽,孙晓静,张丽霞,芦鑫,孟昭建,孙强,黄纪念,张曼玉   

  1. (1.河南省农业科学院农副产品加工研究中心,河南 郑州 450002;2.河南豫研种子科技有限公司,河南 郑州 450002;3.河南农业大学食品科学技术学院,河南 郑州 450002)
  • 发布日期:2020-08-19
  • 基金资助:
    “十三五”国家重点研发计划重点专项(2016YFD0400200);河南省科技攻关计划项目(192102110098;202102110287)

Flavored Peanut Oil Bodies: Optimization of Pretreatment Parameters Based on Fuzzy Mathematic Evaluation and Analysis of Aroma Components

WEI Songli, sun xiaojing, zhang lixia, lu xin, meng zhaojian, sun qiang, huang jinian, zhang manyu   

  1. (1. Research Center of Agricultural Products Processing, Henan Academy of Agriculture Sciences, Zhengzhou 450002, china; 2. Henan Yuyan Seed Co. Ltd., Zhengzhou 450002, China; 3. College of Food Science and Technology, Henan Agricultural University, Zhengzhou 450002, china)
  • Published:2020-08-19

摘要: 基于模糊数学评价法对浓香花生油脂体的9 组预处理参数初步优化,结合气相色谱-质谱联用技术确定浓香花生油脂体的最佳预处理参数,通过主成分分析和正交偏最小二乘-判别分析(orthogonal partial least squares-discriminant analysis,OPLS-DA),探究浓香花生油脂体的香气组成及特征性风味物质。结果表明:140 ℃-30 min组花生油脂体综合评分最高,生腥味轻,特征性香气浓郁且无异味,气相色谱-质谱分析结果与综合模糊评判结果一致,因而确定浓香花生油脂体的最佳预处理参数为140 ℃-30 min;主成分分析和OPLS-DA结果显示,杂环类、醛酮类、醇酚类和其他4 类化合物是影响浓香花生油脂体香气的重要成分,各类别对应的关键特征化合物分别为:2-乙基-6-甲基吡嗪、N-甲基吡咯、2,5-二甲基吡嗪、3-乙基-2,5-二甲基吡嗪、2,3-二氢苯并呋喃、3,5-二乙基-2-甲基吡嗪;苯甲醛、苯乙醛;2-甲氧基-4-乙烯苯酚;1-甲基吡咯-2-羧酸甲酯。

关键词: 浓香花生油脂体;模糊数学评价;香气;主成分分析;正交偏最小二乘-判别分析法

Abstract: Flavored peanut oil bodies prepared with nine combinations of pretreatment parameters (roasting temperature and time) were evaluated by fuzzy mathematic evaluation combined with gas chromatography-mass spectrometry (GC-MS) in order to select the best one. Subsequently, the volatile aroma components of flavored peanut oil bodies and the effects of characteristic compounds on the overall flavor were explored through principal component analysis (PCA) and orthogonal partial least squares discriminant analysis (OPLS-DA). The results showed that the sample with roasting pretreatment at 140 ℃ for 30 min gained the highest comprehensive score, with a light odor of raw peanut and strong characteristic flavor and without off-flavor, indicating good agreement between GC-MS analysis and fuzzy mathematics evaluation. Thus the optimal pretreatment parameters were determined to be 140 ℃ and 30 min. The results of PCA and OPLS-DA showed that heterocyclics, aldehydes and ketones, alcohols and phenols, and other components were the important components affecting the aroma of flavored peanut oil bodies. The key characteristic compounds in the four classes were 2-ethyl-6-methylpyrazine, N-methylpyrrole, 2,5-dimethylpyrazine, 3-ethyl-2,5-dimethylpyrazine, 2,3-dihydrobenzo furan, 3,5-diethyl-2-methylpyrazine; benzaldehyde, phenylacetaldehyde; 2-methoxy-4-vinylphenol; and 1-methylpyrrole-2-carboxylic acid methyl ester, respectively.

Key words: flavored peanut oil bodies; fuzzy mathematic evaluation; aroma; principal component analysis; orthogonal partial least squares-discriminant analysis

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