食品科学 ›› 2023, Vol. 44 ›› Issue (14): 298-304.doi: 10.7506/spkx1002-6630-20220908-076

• 成分分析 • 上一篇    下一篇

橡木片陈酿对柿白兰地风味的影响

李佳敏,孙金旭,王紫娟,袁野,朱会霞,聂馨玙,刘可昕,张一凡,敖常伟   

  1. (1.河北农业大学食品科技学院,河北?保定 071000;2.河北省果蔬发酵技术创新中心,河北?衡水 053000;3.河北农业大学园艺学院,河北?保定 071000)
  • 出版日期:2023-07-25 发布日期:2023-08-11
  • 基金资助:
    河北省科技厅重点研发计划项目(19227141D)

Effect of Oak Chip Aging on the Flavor of Persimmon Brandy

LI Jiamin, SUN Jinxun, WANG Zijuan, YUAN Ye, ZHU Huixia, NIE Xinyu, LIU Kexin, ZHANG Yifan, AO Changwei   

  1. (1. College of Food Science and Technology, Hebei Agricultural University, Baoding 071000, China;2. Hebei Technology Innovation Center for Fruits and Vegetable Fermentation, Hengshui 053000, China;3. College of Horticulture, Hebei Agricultural University, Baoding 071000, China)
  • Online:2023-07-25 Published:2023-08-11

摘要: 以磨盘柿为原料发酵蒸馏制备乙醇体积分数42%的柿白兰地,加入5~20 g/L的国产中度烘烤橡木片进行陈酿。为研究橡木片陈酿的柿白兰地中的各种成分,运用气相色谱-质谱(gas chromatography-mass spectrometry,GC-MS)联用和液相色谱-质谱(liquid chromatography-mass spectrometry,LC-MS)联用分析柿白兰地中的挥发性成分和非挥发性成分的变化,并对添加不同量橡木片柿白兰地的总酚和抗氧化性进行分析,最后进行感官评价。结果表明GC-MS共鉴定出33 种挥发性成分,其中主要成分为乙酸乙酯、癸酸乙酯、月桂酸乙酯,橡木片添加量为10 g/L时,柿白兰地的挥发性成分含量最高;LC-MS鉴定出橡木片陈酿后的柿白兰地中非挥发性物质种类增加了183 种;总酚含量和1,1-二苯基-2-三硝基苯肼(1,1-diphenyl-2-picrylhydrazyl,DPPH)自由基清除能力随着橡木片添加量的增加而增大,陈酿90 d,总酚含量及DPPH自由基清除能力基本稳定;感官评价中,橡木片添加量为15 g/L的柿白兰地得分最高,为72.5 分。

关键词: 柿白兰地;橡木片;挥发性成分;非挥发性成分;总酚;抗氧化性

Abstract: Mopan persimmon brandy with an alcohol content of 42% (V/V), prepared by fermentation and distillation, was aged after being added with 5–20 g/L of Chinese-made moderately roasted oak chips. The volatile and non-volatile components of persimmon brandy were analyzed by gas chromatography-mass spectrometry (GC-MS) and liquid chromatography-mass spectrometry (LC-MS), the total phenol content and antioxidant activity were determined, and sensory evaluation was also performed. The results showed that a total of 33 volatile components were identified by GC-MS, among which the major components were ethyl acetate, ethyl decanoate, and ethyl laurate. The content of volatile components was the highest upon the addition of 10 g/L of oak chips. The results of LC-MS showed that the number of non-volatile substances increased by 183 after aging. The total phenol content and 1,1-diphenyl-2-picrylhydrazyl (DPPH) radical scavenging capacity increased with increasing addition of oak chips, but was basically stable after 90 days of aging. In the sensory evaluation, persimmon brandy with 15 g/L of oak chip scored the highest (72.5 points).

Key words: persimmon brandy; oak chips; volatile components; non-volatile components; total phenolics; antioxidant properties

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