食品科学 ›› 2025, Vol. 46 ›› Issue (23): 257-268.doi: 10.7506/spkx1002-6630-20250617-121

• 成分分析 • 上一篇    

基质极性对真空冷冻干燥香椿含硫特征风味的释放作用

赵丽丽,李怡晴,张合,蒋鹏飞,史冠莹,张乐,史宇婷,靳皓博,张果,肖作兵,王赵改   

  1. (1.河南省农业科学院农产品加工研究中心,河南 郑州 450000;2.河南科技学院食品学院,河南 新乡 453000;3.开封大学,河南 开封 475000;4.上海交通大学农业与生物学院,上海 200000)
  • 发布日期:2025-12-26
  • 基金资助:
    河南省重点研发专项(241111111100);河南省科技攻关项目(252102110081;252102110124); 河南省农业科学院自主创新项目(2025ZC87);河南省农业科学院新兴学科发展专项(2025XK04)

Effect of Matrix Polarity on the Release of Sulfur-Containing Characteristic Aroma Compounds from Vacuum Freeze-Dried Toona sinensis Buds

ZHAO Lili, LI Yiqing, ZHANG He, JIANG Pengfei, SHI Guanying, ZHANG Le, SHI Yuting, JIN Haobo, ZHANG Guo, XIAO Zuobing, WANG Zhaogai   

  1. (1. Agricultural Products Processing Center, Henan Academy of Agricultural Sciences, Zhengzhou 450000, China; 2. School of Food Science, Henan Institute of Science and Technology, Xinxiang 453000, China; 3. Kaifeng University, Kaifeng 475000, China; 4. School of Agriculture and Biology, Shanghai Jiao Tong University, Shanghai 200000, China)
  • Published:2025-12-26

摘要: 以真空冷冻干燥香椿为原料,通过感官评价、电子鼻及气相色谱-离子迁移谱(gas chromatography-ion mobility spectrometry,GC-IMS)、气相色谱-质谱(gas chromatography-mass spectrometry,GC-MS)联用等多维度分析探讨并揭示基质极性对真空冷冻干燥香椿含硫特征风味的释放作用。GC-MS结果发现真空冷冻干燥香椿仅在水处理下能够释放出11 种特征含硫化合物,总量高达(75.26±4.8)µg/g(为新鲜香椿的85.65%),而经过甲醇、乙酸乙酯、环己烷中低极性溶剂处理的真空冷冻干燥香椿中则均不存在特征含硫化合物;电子鼻及GC-IMS结果进一步表明经过水基质处理后的真空冷冻干燥香椿,其气味轮廓和气味组分与新鲜香椿极为相似。本研究明确了高极性基质对真空冷冻干燥香椿中含硫特征风味释放的关键性作用,为干燥香椿独特香气的释放提供了一种新的技术途径,同时对香椿加工产品在多元食品体系中的风味定向调控及应用提供技术支撑。

关键词: 真空冷冻干燥香椿;基质;风味;感官评价;电子鼻;气相色谱-离子迁移谱;气相色谱-质谱

Abstract: In this study, the influence of matrix polarity on the release of characteristic sulfur-containing aroma compounds from vacuum freeze-dried Toona sinensis buds was investigate using sensory evaluation, electronic nose, gas chromatography-ion mobility spectrometry (GC-IMS), and gas chromatography-mass spectrometry (GC-MS). GC-MS results showed that 11 characteristic sulfur-containing compounds were released from the vacuum freeze-dried material after treatment with water, with a total content of (75.26 ± 4.8) µg/g (85.65% of that of fresh T. sinensis). In contrast, these compounds were not detected in the samples treated with solvents of medium to low polarities (methanol, ethyl acetate, or cyclohexane). Furthermore, electronic nose and GC-IMS results indicated that the odor profile and volatile composition of vacuum freeze-dried T. sinensis following water treatment were remarkably similar to those of fresh T. sinensis. This study revealed the crucial role of high-polarity matrices in the release of characteristic sulfur-containing compounds from vacuum freeze-dried T. sinensis. This provides a novel technical approach for releasing the unique aroma of dried T. sinensis and offers technical support for the targeted flavor regulation and application of processed T. sinensis products in multicomponent food systems.

Key words: vacuum freeze-dried Toona sinensis; matrix; flavor; sensory evaluation; electronic nose; gas chromatography-ion mobility spectrometry; gas chromatography-mass spectrometry

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