食品科学 ›› 2008, Vol. 29 ›› Issue (3): 396-399.

• 分析检测 • 上一篇    下一篇

悬浮液进样-火焰原子吸收光谱法测定海产品中铜、铁、锌

 林建原, 徐亚平, 徐金炜, 沈炜熠   

  1. 浙江万里学院生物与环境科学系; 浙江万里学院生物与环境科学系 浙江宁波315100; 浙江宁波315100;
  • 出版日期:2008-03-15 发布日期:2011-08-24

Determination of Copper,Iron and Zinc in Seafood by Flame Atomic Absorption Spectrometry Using Suspension Sample Introduction Technique

 LIN  Jian-Yuan, XU  Ya-Ping, XU  Jin-Wei, SHEN  Wei-Yi   

  1. Department of Biomedical and Environmental Science, Zhejiang Wanli College, Ningbo 315100, China
  • Online:2008-03-15 Published:2011-08-24

摘要: 将海产品样品烘干、粉碎、过筛并悬浮在1.0g/L琼脂溶液中制成悬浮液,以火焰原子吸收光谱法成功地测定了虾、花蛤、牡蛎中铜、铁、锌。对仪器工作条件、悬浮剂稳定性、检出限及加标回收率进行了考察,测定结果的相对标准偏差小于2.7%,测定结果与灰化法一致,相对误差小于±1.5%,其回收率为96.5%~102.3%。此方法简便、快速、准确。

关键词: 悬浮液进样技术, 火焰原子吸收光谱法, 海产品, 铁, 锌,

Abstract: The sample of seafood was bakeout, crushed, sifted and then suspended in 1.0 g/L agar solution, and so made into suspension. Copper, iron and zinc in shrimps, clam and oyster were successfully determined by flame atomic absorption spectrometry. The working condition of apparatus,the stability of suspension, the detection limit and the recovery rate were studied. The relative standard deviations were less than 2.7%. The determination results were consistent with those obtained by ashing method. The relative errors between them were less than±1.5%. The recovery rate lay between 96.5%~102.3%. In FAAS method, the displacement of ashing method by suspension technique for the sample pretreatment of seafood is possible.This method was convenient , speediness and accurate.

Key words: suspension sample introduction technique, flame atomic absorption spectrometry, seafood, copper, zinc, iron