食品科学 ›› 2023, Vol. 44 ›› Issue (21): 121-130.doi: 10.7506/spkx1002-6630-20221007-050

• 食品工程 • 上一篇    

变温烤制对新疆馕坑烤肉色泽、嫩度、杂环胺及多环芳烃含量的影响

魏健, 王莉, 刘飞, 徐泽权, 马欣, 王子荣   

  1. (1.喀什大学生命与地理科学学院,新疆 喀什 844006;2.新疆农业大学食品科学与药学学院,新疆 乌鲁木齐 830052)
  • 发布日期:2023-12-13
  • 基金资助:
    新疆维吾尔自治区自然科学基金项目(2021D01B07);喀什大学科研启动资金项目(ss2016014)

Effect of Variable-Temperature Roasting on the Color, Tenderness, Heterocyclic Amine and Polycyclic Aromatic Hydrocarbon Contents of Xinjiang Nang Pit-Roasted Lamb Meat

WEI Jian, WANG Li, LIU Fei, XU Zequan, MA Xin, WANG Zirong   

  1. (1. College of Life and Geographic Sciences, Kashi University, Kashi 844006, China;2. College of Food Science and Pharmacy, Xinjiang Agricultural University, ürümqi 830052, China)
  • Published:2023-12-13

摘要: 目的:优化新疆馕坑烤肉烤制工艺,研究变温烤制工艺对馕坑烤肉的烤制损失率、色泽、嫩度以及杂环胺(heterocyclic aromatic amines,HAAs)和多环芳烃(polycyclic aromatic hydrocarbons,PAHs)含量的影响。方法:通过L27(36)正交试验结合模糊数学综合评定法优化高温烤制温度(T1)、高温烤制时间(t1)、中温烤制温度(T2)、中温烤制时间(t2)、低温烤制温度(T3)、低温烤制时间(t3)三阶段变温烤制工艺。对比分析高温烤制(high temperature,HT)、低温烤制(low temperature,LT)与变温烤制(CK)馕坑烤肉中HAAs及PAHs含量的差异。结果:变温烤制因素对馕坑烤肉感官评分影响的主次顺序依次为T1>t2>T2>t1>t3>T3,优化工艺组合为T1=300 ℃、t1=4 min,T2=220 ℃、t2=6 min,T3=100 ℃、t3=7 min,感官评分为3.408(满分4 分)。HT、LT、CK组3 种烤制条件下烤制损失率与T2极显著正相关(相关系数r=0.50),剪切力与T1呈显著正相关(r=0.47),肉样内部L*值与t1呈极显著正相关(r=0.57),肉样表层a*值与感官评分呈极显著正相关(r=0.64),肉样表层b*值与烤制损失率呈显著正相关(r=0.40)。HT、LT、CK 3 种烤制条件下生成HAAs总量由高到低依次为HT组>LT组>CK组,CK组最高烤制温度与HT组烤制温度相同,但CK组HAAs总含量显著低于HT组(P<0.05)。LT组与CK组HAAs总量无显著差异(P>0.05)。对HT、LT、CK组HAAs总量进行主成分分析,对主成分1贡献率最高的物质分别为2-氨基-3,4-二甲基咪唑-[4,5-ƒ]喹啉(2-amino-3,4-dimethylimidazo[4,5-ƒ]quinolone,MeIQ)、2-氨基-3-甲基咪唑-[4,5-ƒ]喹喔啉(2-amino-3-methylimidazo[4,5-ƒ]quinoxaline,IQx)、2-氨基-3,7,8-三甲基咪唑-[4,5-ƒ]喹喔啉(2-amino-3,7,8-trimethylimidazo[4,5-ƒ]quinoxaline,7,8-DiMeIQx)。HT组PAHs总含量达(427.45±27.84)ng/g,显著高于LT、CK组(P<0.05);对HT、LT、CK组PAHs总量进行主成分分析,LT组对主成分1、主成分2贡献率最大的物质分别为菲(phenanthrene,Phe)、苯并蒽(benz[a]anthracene,BaA),CK组对主成分1贡献率最大的物质为BaA。结论:该研究优化了馕坑烤肉的变温烤制工艺,发现高温烤制温度是影响变温馕坑烤肉食用品质的关键因素,变温烤制能够有效降低馕坑烤肉中HAAs和PAHs总含量。

关键词: 馕坑烤肉;变温烤制;杂环胺;多环芳烃

Abstract: Objective: The purpose of this study was to optimize the roasting process for Xinjiang Nang pit-roasted lamb meat and explore the effects of variable-temperature roasting on the roasting loss percentage, color, tenderness, and heterocyclic aromatic amine (HAA) and polycyclic aromatic hydrocarbon (PAH) contents of roasted lamb meat. Methods: The three-stage variable-temperature roasting process involving high temperature (T1), roasting time (t1), medium temperature (T2), roasting time (t2), low temperature (T3), and roasting time (t3) was optimized using an L27 (36) orthogonal array design and fuzzy mathematics comprehensive evaluation method. The differences in the contents of HAAs and PAHs in lamb meat roasted at variable temperature (CK), high temperature (HT) and low temperature (LT) were analyzed. Results: The decreasing order of the influence of variable-temperature roasting parameters on the sensory evaluation of roasted lamb meat was as follows: T1 > t2 > T2 > t1 > t3 > T3. The optimal roasting parameters were T1 = 300 ℃, t1 = 4 min, T2 = 220 ℃, t2 = 6 min, T3 = 100 ℃, t3 = 7 min, and the sensory score of lamb meat roasted under these conditions was 3.408 out of 4 points. There was a significant positive correlation between roasting loss percentage and T2 (r = 0.50), between shearing force and T1 (r = 0.47), between internal L* value and t1 (r = 0.57), between surface a* value and sensory evaluation (r = 0.64), and between surface b* value and roasting loss percentage (r = 0.40). The total content of HAAs in roasted lamb meat was in decreasing order of HT > LT > CK. The highest roasting temperature in the CK group was the same as that in the HT group, but the total content of HAAs in the CK group was significantly lower than that in the HT group (P < 0.05). There was no significant difference in the total amount of HAAs between the LT and CK groups (P > 0.05). Principal component analysis of the total amounts of HAAs in the HT, LT and CK groups showed that the substances with the highest contribution rate to the first principal component (PC1) were 2-amino-3,4-dimethylimidazo[4,5-ƒ]quinolone (MeIQ), 2-amino-3-methylimidazo[4,5-ƒ]quinoxaline (IQx) and 2-amino-3,7,8-trimethylimidazo[4,5-ƒ]quinoxaline (7,8-DiMeIQx), respectively. The total content of PAHs in the HT group was (427.45 ± 27.84) ng/g, which was significantly higher than that in the LT and CK groups (P < 0.05). The substances with the largest contribution rate to PC1 and the second principal component (PC2) were phenanthrene (Phe) and benz[a]anthracene (BaA) for the LT group, respectively, and the substance with the largest contribution rate to PC1 were BaA for the CK group. Conclusion: High-temperature roasting temperature is the key factor affecting the eating quality of lamb meat roasted at variable temperature, and variable-temperature roasting effectively reduces the total content of HAAs and PAHs in roasted lamb meat.

Key words: Nang pit-roasted lamb meat; variable-temperature roasting; heterocyclic amines; polycyclic aromatic hydrocarbons

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