食品科学 ›› 2019, Vol. 40 ›› Issue (24): 313-319.doi: 10.7506/spkx1002-6630-20180904-044

• 安全检测 • 上一篇    下一篇

基于气相离子迁移谱检测静电场处理的大菱鲆品质

陈东杰,张明岗,聂小宝,姜沛宏,张玉华,张长峰,任芳   

  1. (1.山东省农产品贮运保鲜技术重点实验室,山东 济南 250103;2.国家农产品现代物流工程技术研究中心,山东 济南 250103;3.潍坊工程职业学院,山东 青州 262500;4.山东海能科学仪器有限公司,山东 德州 251500)
  • 出版日期:2019-12-25 发布日期:2019-12-24
  • 基金资助:
    “十三五”国家重点研发计划重点专项(2018YFD0701000); 山东省重点研发计划项目(2016GGH4526;2017GNC13109)

Quality Detection of Turbot (Scophtalmus maximus) Treated with Electrostatic Field Using Gas Chromatography-Ion Mobility Spectrometry

CHEN Dongjie, ZHANG Minggang, NIE Xiaobao, JIANG Peihong, ZHANG Yuhua, ZHANG Changfeng, REN Fang   

  1. (1. Shandong Key Laboratory of Storage and Transportation Technology of Agricultural Products, Jinan 250103, China; 2. National Engineering Research Center for Agricultural Products Logistics, Jinan 250103, China; 3. Weifang Engineering Vocational College, Qingzhou 262500, China; 4. Shandong Hanon Subsidiary Company, Dezhou 251500, China)
  • Online:2019-12-25 Published:2019-12-24

摘要: 研究静电场对大菱鲆贮藏品质的影响,比较不同贮藏条件下大菱鲆的菌落总数、假单胞菌、总挥发性盐基氮(total volatile base nitrogen,TVB-N)值和硫代巴比妥酸(thiobarbituric acid,TBA)值。采用电子鼻采集其气体指纹信息,通过离子气相迁移谱对不同处理方式大菱鲆的挥发性物质进行分析检测。结果表明:静电场能够改善贮藏期间大菱鲆的品质,有效抑制菌落总数和优势腐败菌的生长及减少TVB-N值和TBA值的增加,在一定程度上抑制了鱼肉内脂肪氧化,具有较好的保鲜效果。采用主成分分析、线性判别分析方法可较好区分不同贮藏时间及不同处理方式的大菱鲆品质。根据气相离子迁移谱采集的指纹图谱,利用热图聚类分析可区分不同贮藏时间内及不同处理方式下大菱鲆挥发性物质。气相离子迁移谱与电子鼻具有快速、准确、无损的特点,可对大菱鲆新鲜度品质进行快速检测可行。

关键词: 大菱鲆, 气相离子迁移谱, 静电场, 品质, 电子鼻

Abstract: The effect of electrostatic field on the storage quality of turbot was studied by examining the changes in total bacterial count (TBC), Pseudomonas aeruginosa count, total volatile basic nitrogen (TVB-N) content and thiobarbituric acid (TBA) value under different storage conditions. The odor fingerprint information was collected by electronic nose and the volatile substances were analyzed and identified by gas chromatography-ion mobility spectrometry (GC-IMS). The results showed that electronic field could significantly preserve the quality of Scophthalmus maximus during storage by inhibiting the growth of TBC and the dominant spoilage bacteria and reducing the increase in TVB-N and TBA values, and suppressed lipid oxidation. The quality of turbot with different storage times and different treatments could be distinguished by using principal component analysis (PCA) and linear discriminant analysis (LDA). According to the GC-IMS fingerprints, the volatile substances of turbot with different storage times and different treatments could be distinguished by heatmap cluster analysis. With the characteristics of rapidity, accuracy and non-destructiveness, the combination of GC-IMS and electronic nose is feasible to detect the freshness and quality of S. maximus.

Key words: Scophthalmus maximus, gas chromatography-ion mobility spectrometry, electronic field, quality, electronic nose

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