食品科学 ›› 2021, Vol. 42 ›› Issue (16): 209-217.doi: 10.7506/spkx1002-6630-20200709-129

• 成分分析 • 上一篇    下一篇

气相色谱-质谱联机结合感官分析共建樱桃香气关联网络

邱爽,唐飞,刘畅,谢美林,魏阳吉,李景明   

  1. (1.中国农业大学食品科学与营养工程学院,北京 100083;2.中化现代农业有限公司,北京 100031)
  • 发布日期:2021-08-27

Aroma Networking of Cherries Based on Gas Chromatography-Mass Spectrometric Data and Sensory Evaluation

QIU Shuang, TANG Fei, LIU Chang, XIE Meilin, WEI Yangji, LI Jingming   

  1. (1. College of Food Science and Nutritional Engineering, China Agricultural University, Beijing 100083, China; 2. Sinochem Agriculture Holdings, Beijing 100031, China)
  • Published:2021-08-27

摘要: 为探究食品香气的仪器分析结果与感官分析结果相结合的策略,挖掘仪器分析在一定程度上替代感官品评的潜力,以9?个不同品种的樱桃样品为试材,分别对其香气进行感官品评及气相色谱-质谱(gas chromatography-mass spectrometry,GC-MS)联用分析,对香气感官品评结果和GC-MS结果计算Pearson相关系数,用以建立二者间的关联网络。根据香气感官品评与GC-MS结果间Pearson相关性得分结果进行偏最小二乘回归(partial least squares regression,PLSR)分析,进一步验证由Pearson相关系数建立关联网络的可靠性。Pearson相关性分析结果及关联网络图均表明樱桃香气感官属性与GC-MS分析结果中多种香气物质显著相关,PLSR分析结果同样表明樱桃香气感官属性中的甜橙味、柠檬味、杏仁味、玫瑰味和酒味均可被GC-MS分析结果解释,证实了根据Pearson相关性分析建立关联网络将香气感官结果与GC-MS结果相结合的可行性。研究认为GC-MS分析作为一种客观、易于标准化的香气评价手段,在水果香气研究中具有一定替代感官分析的潜力。

关键词: 樱桃;香气物质;气相色谱-质谱法;感官品评;关联网络;偏最小二乘回归

Abstract: In order to evaluate the potential of instrumental analysis to replace sensory analysis for food aroma evaluation by combining instrumental and sensory analysis results, the aroma characteristics of nine cherry cultivars were analyzed by gas chromatography-mass spectrometry (GC-MS) and sensory evaluation. The Pearson correlation coefficients between the GC-MS and sensory data were calculated to build an aroma network. According to the Pearson correlation coefficient between the sensory evaluation and GC-MS results, partial least square regression (PLSR) was used to verify the reliability of the established aroma network. The results of Pearson correlation analysis and the aroma network diagram showed that the sensory attributes of cherry aroma were significantly related to a variety of aroma substances identified by GC-MS analysis. Similarly, PLSR analysis showed that the citrus-like, lemon-like, almond-like, rosy and wine-like cherry aroma attributes could be well explained by the results of GC-MS analysis. It was proved that the aroma network was feasible to combine the sensory evaluation results of aroma with the results of GC-MS. It is considered that GC-MS analysis, an objective and easy-to-standardize aroma evaluation method, has the potential to replace sensory analysis in the study of fruit aroma.

Key words: cherry; aroma substances; gas chromatography-mass spectrometry; sensory evaluation; aroma network; partial least squares regression

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