食品科学 ›› 2022, Vol. 43 ›› Issue (6): 265-271.doi: 10.7506/spkx1002-6630-20210419-253

• 成分分析 • 上一篇    下一篇

不同贮藏期冷却滩羊肉煮制后挥发性气味物质的变化

单启梅,罗瑞明,杨波,毕永昭   

  1. (宁夏大学食品与葡萄酒学院,宁夏银川 750021)
  • 出版日期:2022-03-25 发布日期:2022-03-28
  • 基金资助:
    “十三五”国家重点研发计划重点专项(2018YFD0400101)

Changes of Volatile Odor Substances in Chilled Tan Sheep Meat Stored for Different Periods and Cooked

SHAN Qimei, LUO Ruiming, YANG Bo, BI Yongzhao   

  1. (School of Food and Wine, Ningxia University, Yinchuan 750021, China)
  • Online:2022-03-25 Published:2022-03-28

摘要: 为研究不同贮藏期冷却滩羊肉煮制后挥发性气味物质的变化,采用固相微萃取-气相色谱-质谱结合电子鼻技术对0~4?℃不同贮藏期(0、2、4、6、8、10?d)冷却滩羊肉煮制后产生的挥发性气味物质进行测定,并从宏观角度对挥发性气味物质的气味强度进行分析。最终共检测到38?种挥发性气味物质,包括醛类19?种、醇类11?种、酮类4?种、酸类3?种、杂环类1?种,不同贮藏期肉中挥发性气味物质的种类分别为0?d 24?种、2?d 26?种、4?d 30?种、6?d 32?种、8?d 31?种、10?d 29?种,随贮藏期的延长先增加后减少。通过相对气味活度值?(relative odor activity value,ROAV)法确定不同贮藏期冷却滩羊肉煮制后关键香气成分的变化,其中己醛、辛醛、庚醛、(E)-2-辛烯醛、壬醛、苯甲醛、1-戊醇、1-己醇、1-辛烯-3-醇、2-戊基呋喃为不同贮藏期滩羊肉中共有的关键香气成分,其中醛类物质占主导地位,对煮制滩羊肉的风味贡献较大,其ROAV先增大后减小,贮藏至第4天最大。电子鼻测定结果显示贮藏至第4天的冷却滩羊肉经煮制后产生的气味强度较大,煮制滩羊肉的风味较好。

关键词: 滩羊肉;固相微萃取-气相色谱-质谱联用;电子鼻技术;挥发性气味物质

Abstract: The changes of volatile odor substances in chilled Tan sheep meat stored for different periods (0, 2, 4, 6, 8 and 10 days) at 0–4 ℃ and cooked in boiling water were investigated using solid phase micro-extraction (SPME) combined with gas chromatography-mass spectrometry (GC-MS) and an electronic nose system. In total, 38 volatile compounds were detected, including 19 aldehydes, 11 alcohols, 4 ketones, 3 acids and 1 heterocyclic compound. More specifically, the numbers of volatile compounds identified from meat samples stored for 0, 2, 4, 6, 8, and 10 days were 24, 26, 30, 32, 31 and 29, respectively, showing a trend of first increasing and then decreasing with storage period. The key aroma components in cooked meat were identified by relative odor activity value (ROAV). Among them, hexanal, octanal, heptanal, (E)-2-octenal, nonanal, benzaldehyde, 1-pentanol, 1-hexanol, 1-octene-3-ol, and 2-pentyl furan were common to all six samples with aldehydes being the predominant ones, contributing a lot to the flavor of cooked Tan sheep meat. The ROAV of aldehydes increased initially and then decreased, reaching the highest level on the 4th day. The results of the electronic nose showed that cooked four-day stored meat had greater odor intensity and better flavor.

Key words: Tan sheep meat; solid phase micro-extraction combined with gas chromatography-mass spectrometry; electronic nose; volatile odor substances

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